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All Journal Jurnal Riset Kimia EduChemia: Jurnal Kimia dan Pendidikan Dalton : Jurnal Pendidikan Kimia dan Ilmu Kimia Jurnal Pengabdian Magister Pendidikan IPA AL-ULUM: JURNAL SAINS DAN TEKNOLOGI Jurnal Pengabdian Al-Ikhlas Hydrogen: Jurnal Kependidikan Kimia
Antoni Pardede
Program Studi Pendidikan Kimia, FKIP, Universitas Islam Kalimantan, Jl. Adhiyaksa No. 2, Kayu Tangi Banjarmasin, Indonesia 70123
Agriculture, Biological Sciences & Forestry Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Decision Sciences, Operations Research & Management Economics, Econometrics & Finance Education Energy Engineering Health Professions Materials Science & Nanotechnology Social Sciences

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Journal : Jurnal Riset Kimia

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Isolasi Senyawa Metabolit Sekunder Dari Ekstrak Heksana Batang Kelakai (Stenochlaena palustris): Pardede, Antoni; Wardhani, Rr. Ariessanty Alicia Kusuma
Jurnal Riset Kimia Vol. 15 No. 2 (2024): September
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jrk.v15i2.703

Abstract

Isolation is a method of obtaining pure secondary metabolite compounds from plant extracts, which provide benefits such as health, medicine, cosmetics, and agriculture. This research has been carried out and aims to isolate the secondary metabolite compound from the hexane extract of the kelakai stems (Stenochlaena palustris). Phytochemical screening of that extract resulted in a positive-containing steroid. The isolation method includes the separation of hexane extract with column chromatography using silica gel as the stationary phase and eluted successively with hexane, chloroform, and ethyl acetate (step gradient polarity). The column chromatography of the hexane extract resulted in five fractions (H1–H5). Furthermore, fraction H3 was purified to obtain a white needle crystal. The isolated compound spot is invisible in thin-layer chromatography (KLT) under an ultraviolet lamp at 254 nm and 365 nm wavelengths. The isolated compound structure was elucidated by proton and carbon nuclear magnetic resonance (NMR), and mass spectroscopy (MS), as well as comparisons with literature data. The isolated compound is a group of steroids identified as β-sitosterol with the molecular formula C29H50O.
Isolation and Elucidation Structure of the Chemical Component from Ethyl Acetate Subfraction of Kelakai Stems (Stenochlaena palustris) Pardede, Antoni; Wardhani, Raden Roro Ariessanty Alicia Kusuma
Jurnal Riset Kimia Vol. 16 No. 1 (2025): March
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jrk.v16i1.706

Abstract

Kelakai (Stenochlaena palustris) belongs to the Blechnaceae family and offers numerous health benefits due to its chemical components. The isolation and structure elucidation of the chemical components from the ethyl acetate subfraction of the kelakai stems (Stenochlaena palustris) have been carried out. The isolation process began with the preadsorption of 241 mg of the E5.6 subfraction, which was then subjected to separation and purification using column chromatography. Three solvent combinations were used in the process: (chloroform 100%, chloroform: methanol (9:1), and chloroform: methanol (8:2)). The choice of solvent was based on the stain patterns observed in thin-layer chromatography (TLC). The chemical component was successfully isolated after chromatography, resulting in a white needle crystal weighing 15.2 mg and a single spot on the TLC, which was monitored using ultraviolet light at a wavelength of 254 nm. The structure of the chemical component was elucidated using 1H-NMR and 13C-NMR spectra, and comparison with literature data confirmed that the isolated compound from the ethyl acetate subfraction of the kelakai stems is succinic acid.
Co-Authors Akhmad Rizkhi Ridhani Amalia Wahyuni Apriani, Herlina Ariessanty Alicia Kusuma Wardhani Chandra Halim Chandra Halim Chandra Halim Elma Yulida Emilda Frasisca Emilda Prasiska Emilda Prasiska Emilda Prasiska Fauzi, Zainal Fitria Rizkiana Fitria Rizkiana, Fitria Herlina Apriani Herlina Apriani Herlina Apriani Herlina Apriani Herlina Apriani Herlina Apriani Herlina Apriani Herlina Apriani Jarkawi Jarkawi Lusiyana Lusiyana M. Syahriza Finata Mardan Mardan Mardan Mardan Mardan Mardan Mardan Mardan Miftahul Huda Mohan Taufiq Mashuri Muhammad Rasid Rida Nike Nike Norhayani Norhayani Oktaviani Oktaviani Raden Roro Ariessanty Alicia Kusuma Wardhani Rahmah Rahmah Rajak Jamali Riski Novia Syafitri Rr Ariessanty Alicia Kusuma Wardhani Rr Ariessanty Alicia Kusuma Wardhani RR. Ariessanty Alicia K.W Rr. Ariessanty Alicia Kusuma Wardhani Rr. Ariessanty Alicia Kusuma Wardhani Rr. Ariessanty Alicia Kusuma Wardhani Rubi Violeta Sabariah Sabariah Sabariah Sabariah Saribatul Aslamiah Sotikno Sotikno Susilawati Susilawati Susilawati, Susilawati Syafitri, Riski Novia Viony Febriyanti Wahyuni, Amalia Wardhani, Rr Ariessanty Alicia Kusuma Wardhani, Rr. Ariessanty Alicia Kusuma Yasmine Khairunnisa Zainal Fauzi