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All Journal Jurnal Kimia (Journal of Chemistry) Jurnal Ilmu Dasar Microbiology Indonesia IJFAC (Indonesian Journal of Fundamental and Applied Chemistry) Science and Technology Indonesia Jurnal Penelitian Sains Majalah Ilmiah Biologi BIOSFERA: A Scientific Journal PHARMACY: Jurnal Farmasi Indonesia (Pharmaceutical Journal of Indonesia) Seminar Nasional Lahan Suboptimal Molekul: Jurnal Ilmiah Kimia
Elfita Elfita
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Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Control & Systems Engineering Environmental Science Immunology & microbiology Materials Science & Nanotechnology Mathematics Medicine & Pharmacology Physics Other

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Journal : Jurnal Kimia (Journal of Chemistry)

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STUDI REAKSI SIKLOPENTILSILAN DENGAN 4-IODIDA THIOANISOL MENGGUNAKAN KATALIS PALADIUM Aldes Lesbani; Risfidian Mohadi; Elfita Elfita
Jurnal Kimia (Journal of Chemistry) Vol. 7, No. 2 Juli 2013
Publisher : Program Studi Kimia, FMIPA, Universitas Udayana (Program of Study in Chemistry, Faculty of Mathematics and Natural Sciences, Udayana University), Bali, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (278.498 KB) | DOI: 10.24843/JCHEM.2013.v07.i02.p01

Abstract

A study on cyclopentylsilane reaction in tetrahydrofuran with 4-iodo thioanisol has been carried out using palladium as catalyst under argon atmosphere at room temperature. The results showed that the product was tris(4-thioanisyl)cyclopentylsilane (1) which was obtained from recrystallization using methanol with the yield 35%. The Compound (1) has a melting point of 91.5-92.0 oC. Analysis using GC-MS found m/z 466 with six equivalent protons and eight carbons peak obtained from 1H and 13C NMR.
Co-Authors Abd. Rasyid Syamsuri Aldes Lesbani Arsi Arsi Arum Setiawan At panagan At panagan Dachariyanus Dachariyanus Dachriyanus Erise Anggraini Harman Hamidson hasbi hasbi Heni Yohandini Huesin H Bahti Husein Hernadi Bahti IHSAN IVANTRI Julinar Julinar Khodijah Khodijah Marieska Verawaty Mimma Gustianingtyas Muharni Muharni Munawar Munawar Nurlisa Hidayati Risfidian Mohadi Riska Adillah Seni Metasari SITI HERLINDA suparman suparman Supriyatna Supriyatna Suwandi Suwandi