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Journal : Jurnal Sains Materi Indonesia

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Synthesis and Characterization of LaF3:Ce Scintillator Material Sukirman, Engkir; Purwamargapratala, Yustinus; Sugeng, Bambang; Wahyudianingsih, Wahyudianingsih; Gunawan, Indra; Ahda, Syahfandi; Sudjatno, Agus; Dimyati, Arbi
Jurnal Sains Materi Indonesia Vol. 25 No. 1 (2023): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2023.185

Abstract

Synthesis and Characterization of LaF3:Ce Scintillator Material.Synthesis and characterization of the LaF3:Ce scintillator have been carried out. Synthesis was carried out using the co-precipitation method. In this study, the raw materials used were NaF, LaCl3•7H2O, and Ce(NO3)3•6H2O with ethanol and distilled water as a solvent; while surfactants were used oleic acid. In this study, the compound LaF3:0.2Ce was synthesized. The sample was characterized by using an X-Ray Diffractometer (XRD), a Scanning Electron Microscope (SEM), and a Spectrofluorometer. The analyzed data showed that the 82.6 weight fraction of LaF3:0.2Ce phase has precipitated accompanied by the formation of NaCl and C2Ce phases of 5.1 and 12.3 weight fraction, respectively. The NaCl phase is a by-product of the chemical reaction: xLaCl3•7H2O + zCeCl3•7H2O + 3NaF → LaxCezF3 + 3NaCl + 7H2O which could be removed from the precipitate solution by an appropriate separation method, while the C2Ce one appeared as a result of heating the sample at 400ºC. The LaF3:Ce scintillator sample shows the phenomenon of a bluish glow with a lifetime, t = 6 × 10-10 seconds even in the presence of a foreign phase. The existence of NaCl and C2Ce as a local environment still makes LaF3:0.2Ce has normal lifetime characteristics.
Synthesis and Characterization of a Polystyrene-based Scintillator for Gamma Detection Pancoko, Marliyadi; Hafni Lissa Nuri; Manaf, Azwar; Dimyati, Arbi; Jami, Abdul
Jurnal Sains Materi Indonesia Vol. 25 No. 1 (2023): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2023.704

Abstract

This study aimed to create and examine plastic scintillators made from a polystyrene matrix, which are widely used in radiation detection due to their favorable properties such as rapid decay time, low cost, resistance to moisture, and ease of fabrication. The scintillators were doped with p-terphenyl (PTP) and 1,4-bis[2-(phenyloxazolyl)]-benzene (POPOP) using an injection method with an extruder machine. The materials were then characterized using various techniques. Fourier Transform Infrared Spectroscopy (FTIR) revealed the presence of aromatic chains which are essential for the scintillation process. Differential Scanning Calorimetry (DSC) analysis showed stable thermal properties with a glass transition temperature of approximately 100ºC. Scanning Electron Microscopy (SEM) showed that the surface of the polymer is amorphous with small bumps and protrusions likely caused by the PTP and POPOP dopants. The optical evaluation indicated that the sample could absorb UV photons up to 340 nm and emit photons in the wavelength range of 400-500 nm with a peak at 421 nm. Gamma spectra analysis indicated that the plastic scintillators performed well in gamma detection and could be used in a Radiation Portal Monitor (RPM).
Co-Authors Abdul Jami Abu Khalid Rivai Ade, Ade Saputra Agus Hadi Ismoyo Andon Insani Azwar Manaf Bambang Sugeng Bambang Suharno Damar Rastri Adhika Deswita Deswita Engkir Sukirman Ferhat Aziz Hafni Lissa Nuri Huang, Ching An Indra Gunawan Joachim Mayer, Joachim Kusdi Prijono Mardiyanto Mardiyanto Marliyadi Pancoko Marzuki Silalahi Mohammad Dani Nur Rohmat Parikin Parikin Pudji Untoro Putra, Teguh Yulius Surya Panca Riza Iskandar Rohmad Salam, Rohmad RR. Ella Evrita Hestiandari Salim Mustofa Setyo Purwanto Sri Harjanto Sudjatno, Agus Suhendi Suhendi Syahbuddin Syahbuddin Syahfandi Ahda Teguh Yulius Surya Panca Putra, Teguh Yulius Surya Wahyudianingsih, Wahyudianingsih Yustinus Purwamargapratala