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Abdul Malik Karim Amrullah
Universitas Islam Negeri Maulana Malik Ibrahim, Malang
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Journal : Chemistry Indonesian Journal of Chemical Research

 1 
Preparation and Characterization of Cellulose Acetate from Pandanus tectorius via Microwave Irradiation Rizkiana, Meta Fitri; Amrullah, Abdul Malik Karim; Elisah, Nor; Amini, Helda Wika; Palupi, Bekti; Rahmawati, Istiqomah; Fachri, Boy Arief
Indonesian Journal of Chemical Research Vol 12 No 1 (2024): Edition for May 2024
Publisher : Jurusan Kimia, Fakultas Sains dan Teknologi, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598/ijcr.2024.12-riz

Abstract

This research focuses on extracting cellulose from thorn pandan and evaluating its potential as a raw material for cellulose acetate. Thorn pandan contains polysaccharides, especially cellulose. In its fabrication process, cellulose acetate is produced from cellulose acetylation reaction. Cellulose is extracted using the Microwave-assisted Extraction method with variations in NaOH concentration (1, 2, and 3%), H2O2 concentration (10, 20, and 30%), and time variables (20, 40, and 60 minutes). Extraction optimization was performed with Response Surface Methodology (RSM) model BBD (Box-Behken Design). Several characterizations were carried out to determine the characteristics of cellulose acetate, namely Degree of Acetylation, FT-IR spectroscopy and X-Ray Diffraction (XRD). The highest cellulose yield obtained in the extraction process was 50.7% with a variable of 3% NaOH, 30% H2O2 and 60 minutes. XRD analysis shows the angle value 2θ = 22.53798° of thorn pandan cellulose structure is almost similar to commercial cellulose. FTIR functional group identification of cellulose acetate showed the presence of carbonyl (C=O) and (C-O Acetyl) group, respectively seen at wave numbers 1734 cm-1 and 1256 cm-1. The acetyl content of cellulose acetate from thorn pandan produced is 35.475%. Therefore, thorn pandan biomass has the potential as a raw material for making cellulose acetate.
Co-Authors Abdul Bashith Abdul Halim Muhammad Abdul Muntaqim Al Anshory Achmadin, Balya Ziaulhaq Agus Maimun Ahmad Barizi Ahmad Izzuddin Ahmad Jalaludin Ahmad Kholil Ahmad Muhtadi Ridwan Ahmad Sholeh Ahmed Ramdhan Abugren Ahyar Fauzan Al Faruqi, Mhd Ibnu Hannan Anugrah, Audi Anwar, Mohammad Shohibul Arini Elhaq Asbarin Asbarin Audi Anugrah Audina, Noor Amalina Bekti Palupi Berliani, Denitia Boy Arief Fachri Diana Fachrurazi Elisah, Nor Esha, Muhammad In’am Fadzilah, Nurul fanani, zainuddin Fantika Febry Puspitasari Fauziyyah, Eva Ferolisa, Ardhea Fero Haq, Rosyida Rahmatul Harahap, Desi Hariyanti Helda Wika Amini Huda, Ahmad Nawirul Ida Ayu Putu Sri Widnyani Iffatun Najihah Indah Aminatuz Zuhriyah Intan Maulina Isa Ansori Istiqomah Rahmawati Jundatul Afidah Khalilah Ramadhani Khoirudin, Moch. Alfin Lola Hervina H M Arief Affandi Maghfiroh, Rodiatul Maryam Abdullah Kashidan Maulidi Maulidia Meta Fitri Rizkiana Mohammad Asrori Muh. Yunus Muhammad Amin Fathih Muhammad Furqon Almurni Muhammad In'am Esha Muhammad In’am Esha Muhammad Muntahibun Nafis, Muhammad Muntahibun Muhammad Umar Munir, Muhammad Syahrul Muslimin Muslimin Nida, Zahrotun Nidaul Jannah Nofa Isman Novianti, Khusnul Rofida Nur Fausiyah Fadillah Nuril Mufidah NURIL MUFIDAH Nuril Mufidah Nuril Mufidah Nuril Mufidah Putri Restina Dewi Qur'ani, Ainun Suci Rafidatikna, Afifah Ramadhani Lausi Mkumbachi Raqib Alamah Putra Rini Safitri Romadhon, Ahmad Saadatud Darain Saiful Amin Septia Solihati Silvia, Neng Siti Mufarokah Slamet . Sulaikho, Siti Syafi'i, Taqyuddin Ibnu Taqyuddin Ibnu Syafi’i CM Ummah, Khuntum Khaira Uril Baharuddin Uril Bahruddin, Uril Utami, Wiwit Nazilah Waluyo Satrio Adji Wuryaningsih Wuryaningsih Yeni Prihatin Miftahul Jannah Zainuddin Zainuddin Fanani Zenib Mohamed M AlFegeh Zuhri, Muchammad Syaifudin