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Journal : Jurnal Bahan Alam Terbarukan

Extraction and Characterization of Coffee Oil From Instant-Coffee Waste Hanif, Muhammad; Harahap, Fahmi Alif Utama; Heru, Heru; Darni, Yuli; Ginting, Simparmin Br.
Jurnal Bahan Alam Terbarukan Vol 8, No 1 (2019): June 2019 [Nationally Accredited - Sinta 2]
Publisher : Universitas Negeri Semarang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15294/jbat.v8i1.18619

Abstract

The higher demands of fossil energy usage are currently imbalance to its reserves. This issue will give a potency of fossil fuel scarcity that contributes on rising of its cost and disturbing economic stabilization in the future. It is desirable to find another resource which is sustainable and renewable to reduce the dependency on this resource. This study aimed to utilize the oil from instant coffee waste as biodiesel feedstocks. The coffee oil was extracted from instant-coffee waste by Soxhlet extractor and characterized its physical and chemical properties. The solvent extraction through the solid bed of coffee ground performed by five cycles interval using n-hexane as a solvent. Separation processing oil from its hydrocarbon solvent was in a rotary vacuum evaporator and the oil extract collected for further purposes. There was about 17.6% (on a dry weight basis) of coffee oil gained on 20 cycles of extraction. Analysis regarding its physicochemical properties reported that the crude oil has 0.89 g/mL of density, 43.82 mm2/s of kinematic viscosity, 44.47 mg KOH/g of acid value, and 176.40 mg KOH/g of saponification value. The fatty acids composition of the oil provided by GC-MS analyzer showed that unsaturated fatty acids contained, observed as trans-fatty acids rather than cis-fatty acids.
Synthesis of Biofoam from Cassava Peel Starch, Banana Peel Starch and Chitosan as Additives Darni, Yuli; Mayanti, Eva; Anandati, Ghea Maulidaco; Ginting, Simparmin Br.; Lismeri, Lia; Nugrahini, Panca; Utami, Herti
Jurnal Bahan Alam Terbarukan Vol 12, No 2 (2023): December 2023 [Nationally Accredited Sinta 2]
Publisher : Universitas Negeri Semarang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15294/jbat.v12i2.44842

Abstract

Biodegradable Foam (Biofoam) material has been made for application of styrofoam substitute food packaging material from a mixture of starch with chitosan as an additive. The purpose of this study was to determine the effect of molding temperature on biofoam products and to determine the effect of chitosan addition on the physical, mechanical, and biodegrability properties of biofoam made from cassava peel starch (a) and banana peel starch (b) which is close to commercial biofoam standards. The production of biofoam uses variations in molding temperature of 125, 150 and 175 °C and variations in chitosan weight with variations of 0, 1, 2 and 3 grams. The resulting biofoam product was then tested for density, water absorption, compressive strength, biodegradation and functional groups with Fourier Transform Infrared  (FTIR). Based on the results of the study, it is known that biofoam that is close to commercial standards is found in the addition of 3 gr chitosan weight with a molding temperature of 125 °C with a density value of 0.423gr/cm3, water absorption of 42.54% and compressive strength of 0.0045 Mpa. As for biodegradation, biofoam products will decompose 55.17% for 55 days in 0 g chitosan weight with a thermopressing temperature of 175 °C. The spectrum results obtained on biofoam have C-H, C-O, C-N, N-H, C=O and O-H functional groups.
Synthesis of ZSM-5 From Natural Zeolite Lampung (ZAL) and Rice Husk by Seeding Method using Microwaves Ginting, Simparmin Br; Putri, Erisha; Miranda, Thalya; Darni, Yuli; Utami, Herti; Wardono, Herry; Darmansyah, Darmansyah; Rustamaji, Heri
Jurnal Bahan Alam Terbarukan Vol 13, No 1 (2024): June 2024 [Nationally Accredited Sinta 2]
Publisher : Universitas Negeri Semarang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15294/jbat.v13i1.49738

Abstract

ZSM-5 can be synthesized from Lampung Natural Zeolite (ZAL) and rice husks as a source of additional silica. To speed up the synthesis time, ZSM-5 was synthesized using microwaves. Based on this, the synthesis of ZSM-5 was carried out using microwaves at a temperature of 140 oC with a power of 540 watts with time variations of 10, 15 and 30 minutes with the seeding method as a template replacement of 20%. Amorphous silica with a SiO2 content of 95.324% was extracted from rice husks with a suitable alkali solution. The influence of synthesis time on the formation of ZSM-5 has been carried out. The resulting product was characterized using X-ray Diffraction (XRD), and FTIR (Fourier-Transform-Infrared), Scanning Electron Microscopy (SEM) and BET (Brunaur, Emmet and Teller). The results of the analysis show that the results of the research show that the synthesis of ZSM-5 has been successfully carried out by changing the amorphous phase from natural Lampung zeolite and rice husks into ZSM-5 crystals using microwaves which can shorten the synthesis time 216 - 72 times faster than with heating. conventional, produces high crystallinity, provides small particle sizes with larger surface area, pore volume and pore diameter, and microwave radiation does not damage the Si-O bonds. The best sample was obtained at a synthesis time of 30 minutes with a crystallinity percentage of 96.76% and a specific surface area of 138.616 m2 /g.
Co-Authors Achmad Ariyadi Adisaputro, Jonathan Kristian Agustina Iryani, Dewi Anandati, Ghea Maulidaco Arya Perdana, Guntur Aviati S., Yuniar Azhar Azhar Azhar Azhar Azhar Azizah, Ara Annastasya Azlia Metta Azlia Metta Badaruddin, M. Damaru, Restu Damayanti, Sri Ismiyati Darmansyah Darmansyah . DARMANSYAH . Darmansyah . Darmansyah Darmansyah Darmansyah Darmansyah Devi Permata Sari Devianto, Hary Dewi Agustina Iryani Dewi Agustina Iryani Dewi Agustina Iryani Dewi Agustina Iryani, Dewi Agustina Donny Lesmana Donny Lesmana Dwi Derti Sulistiowati Elida Purba Elistia Nursafitri Febriyanto, Pramahadi Feerzet Achmad Guntur Arya Perdana Harahap, Fahmi Alif Utama Harahap, Katrina Hens Saputra Hens Saputra Heri Rustamaji Heri Wardono Hermiyati, Ria Putri Hermiyati, Ria Putri Herry Wardono Herti Utami Herti Utami Herti Utami Herti Utami Heru, Heru Islamia, Ulfa Jonathan Kristian Adisaputro lialismeri Lismeri, Lia M. Haviz M. Praditia Ansor M. Yassien Nurfiqih Mardhotillah, Nur Anisa Marlina, Arlin Mayanti, Eva Miranda, Thalya Muhammad Hanif Muhammad Hanif Muhammad Haviz Nabilla Uliane Ni Luh Gede Ratna Juliasih Nisa Meutia Risthy Novaringga, Adellia Nugrahini, Panca Nur Arifaini Nur Hasanah Nurhasanah Husin Otik Nawansih Pandiangan, Kamisah Delilawati Pista, Annisa Fitria Puligadda, Lohit Krishna Pranav Putri, Erisha Putri, Yolanda Dwika Putriani, Eka Nanda Ria Putri Hermiyati Risthy, Nisa Meutia Sebastian Djoni Syukur Sebastian Djoni Syukur Silviyanti, Serly Siti Nurul Khotimah Solly Aryza Sri Ismiyati Damayanti Sujoto, Vincent Sutresno Hadi Sulistiowati, Dwi Derti Sulistiowati, Dwi Derti Taharuddin Taharuddin Thalya Miranda Tirto Prakoso Ulfa Islamia Vincent Sutresno Hadi Sujoto Widi Astuti Widiatmoko, Pramujo Yeni Yulia Yeni Yulia Yolanda Dwika Putri Yuli Darni Yuli Darni Yuli Darni Zulaikha Setya Mega Sari