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All Journal JURNAL KIMIA SAINS DAN APLIKASI KOVALEN: Jurnal Riset Kimia Jurnal Sains dan Teknologi Pangan Jurnal Progres Kimia Sains Jurnal Penelitian Pendidikan IPA (JPPIPA) Chemistry Indonesian Journal of Chemical Research Jurnal Ilmu Kefarmasian Indonesia Sarwahita : Jurnal Pengabdian Kepada Masyarakat Cokroaminoto Journal of Chemical Science Jurnal Mandala Pengabdian Masyarakat Jurnal Akademika Kimia Amal Ilmiah: Jurnal Pengabdian Kepada Masyarakat Jurnal Akademika Kimia Jurnal Analis Kesehatan Kendari
THAMRIN AZIS
UNIVERSITAS HALU OLEO
Agriculture, Biological Sciences & Forestry Humanities Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Education Energy Engineering Environmental Science Health Professions Immunology & microbiology Materials Science & Nanotechnology Medicine & Pharmacology Physics Public Health Social Sciences Other

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Journal : Jurnal Akademika Kimia

 1 
Synthesis and Characterization of Activated Carbon from Waste Compedak Fruit (Artocarpus Champeden) Activated H3PO4 as Adsorbent of Methylene Blue Catherina Bijang; Matheis F. J. D. P. Tanasale; Dewi Sri; Tahril Tahril; Thamrin Azis
Jurnal Akademika Kimia Vol. 11 No. 1 (2022)
Publisher : Universitas Tadulako

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/j24775185.2022.v11.i1.pp56-63

Abstract

Synthesis of activated carbon from cempedak peel waste is carried out to utilize biomass waste. This study aimed to synthesize and characterize activated carbon from cempedak peel waste. The synthesis was carried out by chemical activation using phosphoric acid with a dry impregnation ratio of 1:4 (g sample:g H3PO4). Samples impregnated for 24 hours were then heated at 250℃—and then calcined at 350℃ and 450℃. The XRD and FTIR characterization results indicated that the activated carbon obtained had an amorphous structure and the activated carbon obtained had hydroxyl, carbonyl, and carboxylic groups. Activated carbon with the highest yield was obtained at a temperature of 350, namely 43%. The results of determining the water content of activated carbon obtained are 8.36% at 350 0C and 7.1% at 450 ℃. The value of water content and ash content of activated carbon from the skin of this cempedak fruit has met the Indonesian National Standard (SNI 06-3730-1995). The best-activated carbon yield was at a calcination temperature of 450, with the percentage of adsorption efficiency on methylene blue of 98.88%.
Equilibrium and Adsorption Kinetic Study of Metal Ni(II) using Persimmon Tannin Gel La O. Ahmad; Ulfa H. Syam; Laode A. Kadir; Nohong Nohong; Muh Natsir; Nasriadi Dali; Imran Imran; Tahril Tahril; Thamrin Azis
Jurnal Akademika Kimia Vol. 11 No. 2 (2022)
Publisher : Universitas Tadulako

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/j24775185.2022.v11.i2.pp111-116

Abstract

Heavy metal concentration exceeding the threshold amount is hazardous to the environment, so it needs some treatment. The study aimed to know the capacity and kinetics of adsorption. This study used the adsorption method to remove the heavy metal ion Ni(II) using persimmon tannin gel. Influences of time contact, pH, and ion concentration in the adsorption process were also investigated. Results showed optimum adsorption at 60 minutes of time contact and pH 5. Variation of concentration made the adsorption decrease as metal ion Ni(II) concentration increased. The maximum adsorption capacity was 23.14 mg/g by using pseudo-second-order adsorption kinetic model.
Performance of The Composite Electrode of Reduced Graphene Oxide Palm Oil Shell - Zinc Oxide (rGOCKS - ZnO) as a Chemical Oxygen Demand (COD) Sensor by Photoelectrocatalysis Azis, Thamrin; Muzakkari, Muhammad Z.; Nurdin, Muh.; Maulidiyah, Maulidiyah; Muslia, Wa O.; Bijang, Catherina M.; Tahril, Tahril
Jurnal Akademika Kimia Vol. 12 No. 2 (2023)
Publisher : Universitas Tadulako

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/j24775185.2023.v12.i2.pp123-131

Abstract

The preparation of reduced graphene oxide composite electrodes from palm shells (rGOCKS-ZnO) as a chemical oxygen demand (COD) sensor by photoelectrocatalysis has been successfully carried out. The preparation of rGOPS - ZnO electrodes by thermal reduction method and modified Hummer. The XRD results showed several peaks of rGOCKS - ZnO namely 23.287 º, 26.781 °, 29.889 °, 32.468 °, 35.109 °, 37.14 °, 39.822 °, 43.559 °, 47.927 °, and 48.537 °. SEM-EDX analysis reveals the surface of graphene sheets containing aggregates in the shape of small particles attached to graphene sheets. The results of the EDX analysis consisted of C 67.82 %, O. 19.2 %, Zn. 7.85 % and 5.13 % impurity. The CV and LSV tests showed that the rGOAK - ZnO electrode with a variation of 1 gram: 0.3 gram had a good response to the oxidation process under visible light. The profile tests of these organic dyes (methylene blue) in concentrations of 0.5 ppm, 1.0 ppm, 2.0 ppm, and 3.0 ppm were applied by Multi Pulse Amperometry (MPA). The performance of the rGOPS - ZnO electrode has been in determining the value of COD by photo electrocatalytic good sensitivity, linearity, limit of detection, repeatability, and service life. The COD value was determined using the rGOPS - ZnO electrode and obtained 2.97897 mg/LO2 close to the theoretical value.
Synthesis of Silver Nanoparticles using Gandaria Seeds Bioreductor Bijang, Catherina M.; Hasanela, Nurani; Joris, Shielda N.; Fransina, Eirene G.; Tahril, Tahril; Azis, Thamrin; Tehuayo, Ahmadin
Jurnal Akademika Kimia Vol. 12 No. 2 (2023)
Publisher : Universitas Tadulako

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22487/j24775185.2023.v12.i2.pp142-148

Abstract

The silver nanoparticles (NPP) are synthesized with the chemical reduction method by using a water extract bioreductor of gandaria seed (Bouea macrophylla G.) which acts as a reducing precursor, in this case, AgNO3 Ag+ is reduced to AgO. The concentration of AgNO3 is made between 0.5 mm and 1 mm. The characteristic of NPP is unstable, so a modification is needed with and without the addition of PVA 1 %. The process of NPP shaping is monitored by observing the uptaken of UV - Vis when the color changes occur. The high NPP concentration of AgNO3 has higher absorbance and is wider if compared to the lower AgNO3 concentration. The result of this research based on the absorbance value and the wavelength showed the NPP synthesized without the addition of PVA 1 % (b/v) is wider. The addition of PVA 1 % (b/v) provides better stability and maintains the absorbance of spectrum changes from day to day. The maximum uptaken of UV-Vis from NPP AgNO3 0.5 mm by using green synthesis and 1 mm without adding PVA are 0.946 and 0.980, respectively. However, NPP with the addition of PVA has 0.968 and 0.978 absorbance. The best concentration of NPP produced was 1 mm AgNO3.
Co-Authors A. Nurwahida Aceng Haetami, Aceng Aden Mula Pratiwi Alimin Alwahab Alwahab Amalia, Fajri Fitra Angga Febrian Bijang, Catherina M. C Bijang C Bijang Caterina Bijang Catherina Bijang Dewi Sri Dewi, Dian Puspita Dian Permana Fajrin E. Rosa Fransina, Eirene G. Haris W Hasanela, Nurani Holilah Holilah, Holilah I Wayan Sutapa Imran Imran Imran Imran Imran Irwan Irwan Joris, Shielda N. Juwita, Citra Kadir, La Ode Abd Keke Awaliyah Kelrey, Adhi G. La Aba La Agusu La O. Ahmad La Ode Abd Kadir La Ode Abd Kadir La Ode Abd Kadir La Ode Ahmad La Ode Kadidae, La Ode La Ode Santiaji Bande La Rudi Laily Nurliana Laily Nurliana Laode A. Kadir Laode A. Kadir Laode Abdul Kadir Laode Abdul Kadir M. Natsir Mansur, Inda Ulfa Matheis F. J. D. P. Tanasale Maulidiyah Maulidiyah Maulidiyah Maulidiyah Maulidiyah Maulidiyah Maulidiyah MAULIDIYAH MAULIDIYAH Muh Natsir Muh. Natsir Muh. Natsir Muh. Natsir Muh. Nurdin Muh. Nurdin, Muh. Muh. Zakir Muzakkar Muhammad Nurdin Muhammad Nurdin Muhammad Nurdin Muhammad Nurdin Muhammad Zakir Muzakkar Muhammad Zakir Muzakkar Muslia, Wa O. Muzakkar, Muhammad Zakir Muzakkari, Muhammad Z. Nasriadi Dali Nasriadi, Nasriadi Nohong Nohong Nohong Nohong Nohong Nohong, Nohong Nur Illyyin Akib Nurhaeni R, Halimatussaddiyah Ratna Ratna Ratna Ruslan Ruslan Ruslan Ruslin Ruslin Sahidin SITTI HADIJAH SABARWATI Sitti Ratna Sri Wahyuni Syahrir T Nurwahida Tahril Tanasale, M.F.J.D.P. Tehuayo, Ahmadin Ulfa H. Syam Viesta Valentin Octavian Wa Ode Harlis Wiwik Handayani Yodha, Agung Wibawa Mahatva Zainal Syam Arifin Zul Arham