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Journal : Jurnal Riset Fisika Indonesia

Sintesis dan Karakterisasi Silika Gel dari Limbah Botol Kaca sebagai Adsorpsi Ion LOgam Berat (Pb) pada Air Pasca Tambang (Kolong) di Bangka Livia Livia; Widodo Budi Kurniawan; Dewi Marina; Sitti Patimah Wati
Jurnal Riset Fisika Indonesia Vol 1 No 1 (2020): Desember 2020
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (330.831 KB) | DOI: 10.33019/jrfi.v1i1.1988

Abstract

Glass bottle waste is inorganic waste that cannot be broken down by microorganisms. The high SiO2 content in glass bottle waste has the potential as a base material in the synthesis of silica gel. This study aims to determine the characteristics and ability of silica gel as adsorption of Pb metal ions in water under Bangka. The stages in this study were started from the extraction of silica from waste glass bottles, synthesis of silica gel, activation with HCl and testing the adsorption of Pb metal ions in under water. The results showed that the characteristics of silica gel with variations of 100 and 200 mesh, the concentration of 3M NaOH, 3M HCl using SEM EDS had an amorphous structure and the SiO2 content graph had high peaks. In the BET test, the pore radius was 1164.207 for the 100 mesh sample and 1293.102 for the 200 mesh sample. The AAS results showed that in the treatment of 100 mesh, the Pb value decreased by -0.1122, while for 200 mesh also decreased by -0.1322. The Pb value is minus because the tool can only read with a standard limit of 0.1. If it is less than 0.1, then the tool cannot read the value on Pb metal even though the value is minus but has a value. The greater the minus, the lower the Pb value. So silica from glass bottle waste can adsorb heavy metals (Pb) on the surface water underneath
Perangkat Penyimpanan Muatan Listrik Ramah Lingkungan Berbasis Karbon Aktif Dari Limbah Hasil Pengolahan Muntok White Pipper Ipi Ipi; Aisyah Deri Ayu Tungga Safitri; Yunita Febriani; Widodo Budi Kurniawan; Megiyo Megiyo
Jurnal Riset Fisika Indonesia Vol 2 No 1 (2021): Desember 2021
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (500.835 KB) | DOI: 10.33019/jrfi.v2i1.3017

Abstract

The national need for advanced materials is spread across several fields, such as industry, transportation, information systems and military defense systems. In the field of transportation, the government continues to innovate by shifting fuel-based vehicles (BBM) towards environmentally friendly cars in the form of electric cars. However, the main challenges in developing this electric car are the electric energy charge storage system which is durable, has high storage capacity, and short charging time. In this study, carbon was activated gradually using a 7% H3PO4 solution followed by heating at a temperature of 700oC for 3 hours under nitrogen gas (N2). The results of the FTIR analysis showed that the activated carbon N2 gas had a strong and sharp C=C group along the absorption band 1500 cm-1 – 1400 cm-1 which indicated that the activated carbon had high quality and purity. This result was strengthened based on the EDS spectra which showed a carbon content of 90.56%. In addition, based on SEM micrographs, it can be observed that the morphology of the carbon produced has pores scattered on the surface. The presence of these pores will provide space for the transfer of charge or ions to the electrode. The best electrode was obtained on activated carbon with N2 gas activation treatment with a conductivity of 3.92 x 10-2 S/m and a capacitance of 1.44 x 10-3 F, so it was concluded that activated carbon muntok white paper can be used as an electric charge storage material.
Karakteristik Karbon Aktif Limbah Kulit Lada (Piper Nigrum L) sebagai Elektroda Superkapasitor Dewi Marina; Widodo Budi Kurniawan
Jurnal Riset Fisika Indonesia Vol 2 No 1 (2021): Desember 2021
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (571.583 KB) | DOI: 10.33019/jrfi.v2i1.3171

Abstract

Pemenuhan kebutuhan energi dibutuhkan suatu piranti penyimpan yang memiliki kapasitansi spresifik yang tinggi yaitu superkapasitor. Superkapasitor adalah perangkat penyimpan muatan yang memiliki kapasitansi spesifik yang tinggi. Dalam penelitian ini telah dilakukan preparasi dan karakterisasi karbon aktif dari limbah kulit lada sebagai bahan elektroda superkapasitor. Karbon diaktivasi dengan variasi aktivator NaOH 1 M, 3 M dan 5 M dilanjutkan dengan pemanasan pada suhu 700˚ C selama 3 jam dengan dialiri gas nitrogen (N2). Karbon selanjutnya dikarakterisasi menggunakan Scanning Electron Miscroscopy-Energy Dispersive Spektroscopy (SEM-EDS), Brunauer-Emmett-Teller (BET) dan pengukuran kapasitansi menggunakan metode Cyclic Voltametry (CV). Hasil pengujian menunjukkan karbon aktif limbah kulit lada berpori dengan bentuk pori bulat pada sampel 3 M dan 5 M, sedangkan pada 1 M terdapat pori berongga yang pipih dan panjang. Hasil EDS setiap sampel memiliki kandungan unsur karbon (C) secara berurut yaitu 77,57%, 75,96%, dan 74,62%. Hasil BET menunjukkan luas permukaan maksimum sebesar 149,319 m2/g. Kapasitansi elektroda superkapastitor tertinggi diperoleh pada konsentrasi 5 M dengan laju scan 1 mV/s yaitu 12,68 F/g.
Identifikasi Sebaran Air Lindi (Leachate) Menggunakan Metode Geolistrik Self-Potential (SP) Di Tempat Pembuangan Akhir (TPA) Parit Enam Kota Pangkalpinang Hoirotul Padilah; Yekti Widyaningrum; Widodo Budi Kurniawan
Jurnal Riset Fisika Indonesia Vol 2 No 1 (2021): Desember 2021
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1157.708 KB) | DOI: 10.33019/jrfi.v2i1.3208

Abstract

Garbage is a common pollutant that causes various negative impacts such as lack of aesthetic value to the environment, brings various types of diseases and clogs waterways. The waste is then transported and disposed of at the TPA. The Parit Six TPA in Pangkalpinang City accommodates around 150 tons of garbage every day. This will cause contamination of water, soil and ground water by leachate seeping from the pile of garbage exposed to rain. The leachate can be identified using the Geoelectric Self Potential (SP) method using a fixed base technique with a space between the electrodes of 5 m. Then obtained the results of data acquisition from 6 paths as many as 92 points. Furthermore, the resulting data will be corrected and processed to produce isopotential contours and topography. Based on isopotential contours and topography, the distribution of fluid in the area around the Parit Enam TPA Pangkalpinang City is spread in the northeast, southwest to the north of the study area. The fluid quality around the study site is known from the results of density and pH of the sample well water. These results show the distribution of leachate in the area around the Parit Enam TPA Pangkalpinang City is spread from the northeast to the southwest in the northern part of the research area and from the southwest to the southern part of the research area towards the northern part of the research area.
Uji Linieritas Kalium Tiosianat (KSCN) Sebagai Indikator Kolorimetri Untuk Mendeteksi Konsentrasi Fe Pada Air Azrul Fahmi; Widodo Budi Kurniawan; Anisa Indriawati
Jurnal Riset Fisika Indonesia Vol 2 No 2 (2022): Juni 2022
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (435.582 KB) | DOI: 10.33019/jrfi.v2i2.3215

Abstract

The method of testing water quality that is in great demand by researchers because it is practical and inexpensive, one of which is the colorimetric method. To detect the concentration of Fe using a colorimetric method used a colorimetric indicator such as potassium thiocyanate (KSCN). KSCN is a compound consisting of the elements potassium (K), sulfur (S), carbon (C), and nitrogen (N) which can produce an orange color when reacted with Fe. In this study, 20 variations of Fe solution were used with a concentration difference of 0.5 ppm starting from 0.5 ppm to 10 ppm and obtained a correlation coefficient of 0.9962 through the UV-Vis spectrophotometer test so that potassium thiocyanate (KSCN) can be used as a colorimetric indicator for detect the concentration of Fe in water.
Synthesis And Characterization Of Carbon-Chitosan Composite Electrodes Based On Biomass Carbon Activated Using The Microwave Method Deden Nurdandi; Herman Aldila; Widodo Budi Kurniawan
Jurnal Riset Fisika Indonesia Vol 2 No 2 (2022): Juni 2022
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (535.264 KB) | DOI: 10.33019/jrfi.v2i2.3216

Abstract

In this research, the synthesis and characterization of chitosan modified carbon composites based on biomass carbon has been carried out using the microwave method. Chemically activated carbon with 2.5% H3PO4 activator was stirred using a magnetic stirrer for 1 hour and allowed to stand for 24 hours. The carbon was then physically reactivated using a microwave for 20 minutes with a power variation of 800, 1000 and 1200 watts and a Scanning Electron Microscopy (SEM) test was carried out. After the SEM test, chitosan modified carbon was synthesized with a composition ratio of 1:1, 2:1 and 3:1 and the specific capacitance was measured using Galvanostatic Charge-Discharge (GCD) testing. The SEM test results analyzed using ImageJ software-based image processing methods show that the value of sphericity, pore size and carbon porosity decreases with increasing microwave power used. The optimum conditions based on the value of Sphericity, pore size and porosity were obtained at a variation of 800 watts of microwave power with values ​​of 0.952, 0.832 m, and 25.87%, respectively, which were included in the macropore size (>50 nm). Because the higher the power used, the smaller the pore area and porosity. The electrode-specific capacitance values ​​were 3.4 x 10-1 F/g, 24.02 F/g, and 1.3 x 10-1 F/g, respectively. Electrodes with a ratio of 2:1 have the largest capacitance value, because they can be charged by an electric charge. The longer the charge-discharge process, the greater the capacitance value, so the curve will approach a more symmetrical isosceles triangle shape.
The Effect Of Contact Time Variations On The Efficiency Value And The Adsorption Kinetic Mechanism Of Iron (Fe) On Batik Waste Cual Using Chitosan Widodo Budi Kurniawan; Herman Aldila; Livia Livia
Jurnal Riset Fisika Indonesia Vol 2 No 2 (2022): Juni 2022
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (391.677 KB) | DOI: 10.33019/jrfi.v2i2.3221

Abstract

English
Sintesis dan Karakteristik CaCO3 dari Cangkang Kerang Kepah (Polymesoda erosa) sebagai Doping Anoda Baterai Lithium-Ion Yunior Trisakti; Lizia Miratsi; Widodo Budi Kurniawan
Jurnal Riset Fisika Indonesia Vol 3 No 1 (2022): Desember 2022
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33019/jrfi.v3i1.3548

Abstract

Synthesis and Characteristics of CaCO3 from Kepah Clam Shells (Polymesoda erosa) as Anode Doping of Lithium-Ion Batteries LTO (Lithium Titanate Oxide) or Li4Ti5O12 is one of the candidates for graphite replacement anode material in the production of Lithium-ion batteries. However, LTO materials have the disadvantage of low electrical conductivity, which limits the working level of the battery. Kepah clam shells are one of the wastes that have not been widely used even though the amount is still very abundant, and is expected to have the potential to be in the source of CaCO3 because it contains high amounts of calcium. Therefore, this study aims to determine the content of CaCO3 in the shell of the kepah clam (Polymesoda erosa) and determine the conductivity value of the LTO anode doped with CaCO3 of the kepah clam shell. The synthesis method used is the solid state reaction method with variations in doping concentrations of 0.00 mol, 0.10 mol, 0.15 mol, and 0.20 mol. The results of XRF analysis on the shell powder showed that the most dominant element content was Ca which was 97.63%. So it shows that calcium carbonate (CaCO3) from the shells of kepah mussels was successfully prepared. Furthermore, the anode active material was obtained, which if obtained XRD results and analyzed would show the absence of the CaCO3 phase, and there was no doping influence, then the active material powder was synthesized Li4Ti5O12 anode sheet doped CaCO3 shell. As for knowing the conductivity value of the Li4Ti5O12 anode sheet doped by CaCO3 clam shells, it is further characterized using Electrochemical Impedance Spectroscopy (EIS).
Sintesis Teori A dan B sebagai Upaya Menjelaskan Inonsistensi Teori C dalam Proses Agitated Leaching Tailing Timah Muhammad Sahroni; Anisa Indriawati; Widodo Budi Kurniawan
Jurnal Riset Fisika Indonesia Vol 3 No 2 (2023): Juni 2023
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33019/jrfi.v3i2.4125

Abstract

Inkonsistensi teori C merupakan anomali dimana teori C tidak berlaku dalam proses Agitated Leaching. Hal ini menuntut penjelasan sehingga banyak peneliti berspekulasi untuk menjelaskannya. Contohnya teori A yang kontra- intuitif dan teori B yang cenderung menentang teori A. Dalam penelitian ini telah dilakukan penyelidikan terhadap teori A dan B melalui pendekatan tidak-langsung dengan variabel terikat dari proses Agitated Leaching adalah Total Dissolved Solid (TDS), laju pengadukan sebagai variabel bebas dan variabel tetap adalah rasio solid-likuid (1:20 Gr/mL) dan lama pengadukan (10 menit). Proses pelaruran dilakukan pada keadaan STP dan membatasi proses hanya pada tahap pelarutan sampel menggunakan HNO3 5%. Sampel yang digunakan adalah pasir tailing timah. Hasil penelitian menunjukkan bahwa inkonsistensi terjadi pada laju pengadukan 1000 rpm. Teori A1 tidak dapat disimpulkan keberlakuannya dalam proses pelindian tailing timah. Teori A2 berlaku dalam proses pelindian tailing timah. Teori B berlaku dalam proses pelindian tailing timah.
Pengaruh Penambahan Karbon Aktif Dari Kulit Lada dan Suhu Aktivasi Karbon terhadap Nilai Konduktivitas Anoda Berbasis LTO Jefri Akbar; Widodo Budi Kurniawan; Yekti Widyaningrum; Anisa Indriawati
Jurnal Riset Fisika Indonesia Vol 4 No 1 (2023): Desember 2023
Publisher : Jurusan Fisika, Universitas Bangka Belitung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33019/jrfi.v4i1.3823

Abstract