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Determining Crystallite Size Using Scherrer Formula, Williamson-Hull Plot, and Particle Size with SEM Made Sumadiyasa; I.B.S. Manuaba
BULETIN FISIKA Vol 19 No 1 (2018): BULETIN FISIKA
Publisher : Departement of Physics Faculty of Mathematics and Natural Sciences, and Institute of Research and Community Services Udayana University, Kampus Bukit Jimbaran Badung Bali

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Abstract

It has been determined the crystallite size by XRD technique using Scherrer equation and Williamson-Hull Plot method. While the particle size is determined by SEM using Image-J software. For this purpose, synthesized samples of compound Gd0,95La0.05Ba2Cu3O7-d phase. From the calculation results, obtained the crystallite size in nanometers order, however the crystallite size resulting from the Scherrer equations and Scherrer Modified is different, i.e. 63.1675 nm and 67.0005 nm. The results of the crystallite size calculation by the scherrer equation directly and modified differed from that of the Williamson-Hull Plot method (97,3040 nm). Meanwhile, the results of the Williamson-Hull Plot methods and SEM show almost the same value (98.7297nm).
The effect of various disturbances on the seeds on the content of chlorophyll a, chlorophyll b, carotenoids, and biomass of cayenne pepper Seedlings Ni Nyoman Rupiasih; Ni Kadek Gita Hari Yanti; Made Sumadiyasa; I.B.S. Manuaba
BULETIN FISIKA Vol 19 No 1 (2018): BULETIN FISIKA
Publisher : Departement of Physics Faculty of Mathematics and Natural Sciences, and Institute of Research and Community Services Udayana University, Kampus Bukit Jimbaran Badung Bali

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Abstract

Study on the effect of various disturbances on the cayenne pepper seeds (Capsicum Frutescens L.) to the content of chlorophyll a, chlorophyll b, carotenoids, and biomass of the plants in the germination period have been done. The disturbances given include UV-C irradiation for 1 hour (S1), microgravity for 12 hours (S2), for 24 hours (S3), and for 48 hours (S4), as well as combined disturbances that are UV-C irradiation for 1 hour followed by microgravity for 12 hours (S5), for 24 hours (S6), and for 48 hours (S7). As comparison, it has been used seeds without treatment called control (S0). The microgravity environment was created using a 2-D clinostat with a rotational speed of 2.7 rpm (1.2 x 10-4 g). All samples were grown in normal gravity (1 g) environment. Observations were made during the vegetative phase until the plant was 40 days old. Measurements of chlorophyll a, chlorophyll b, carotenoids, and biomass were performed at the plants were 10, 20, and 40 days old. The results showed that disturbances which given on the seeds gave positive effects on the content of chlorophyll a, chlorophyll b, carotenoids, and biomass of the plants. The impacts depend on the duration of the disturbances given.