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All Journal SAINSMAT SMART: Jurnal Pengabdian Kepada Masyarakat
Suriati Eka Putri
Universitas Negeri Makasar
Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Education Environmental Science Physics Social Sciences Other

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Microstructure Investigations of Natural Clay From Pattallassang District, Takalar Regency, South Sulawesi Province, Indonesia Abd Rahman; Suriati Eka Putri; Diana Eka Pratiwi; Satria Putra Jaya
Sainsmat : Jurnal Ilmiah Ilmu Pengetahuan Alam Vol 12, No 1 (2023): Maret
Publisher : Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Negeri Makassar

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35580/sainsmat121444522023

Abstract

The study aimed to investigate the microstructure of natural clay from Pattallassang District, Takalar Regency, South Sulawesi Province. The clay was characterized using X-ray diffractometer (XRD), surface area analyzer (SAA), and scanning electron microscope (SEM). The XRD analysis showed that the main mineral composition of the clay was kaolinite, quartz, hematite, geothite, magnetite, and anatase phases. The SAA using BET analysis shows the large surface area of 59.26 m2/g and BJH analysis for pore distribution of 32.77 nm. SEM observations revealed that the clay consists of plate-like kaolinite particles arranged randomly. The results indicate that the natural clay from Pattallassang District has good potential for use in various industrial applications due to its high kaolinite content and favorable microstructure.Keywords: kaolinite, microstructure, mineral, clay.
The Effect Of Acid Treatment On The Characteristics Of Modernite Zeolite Sumiati Side; Suriati Eka Putri; Diana Eka Pratiwi; Aulia Rahma; Abd. Rahman
Sainsmat : Jurnal Ilmiah Ilmu Pengetahuan Alam Vol 12, No 2 (2023): September
Publisher : Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Negeri Makassar

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.35580/sainsmat122511932023

Abstract

This work investigated the use of acid treatment on the characteristics of zeolite mineral. The effects of treating zeolite with various acid solutions hydrochloric acid (HCl) and sulfuric acid (H2SO4) were measured using x-ray fluorescence (XRF), x-ray diffraction (XRD), and scanning electron microscope (SEM). The results showed an increase in the percentage of SiO2 and Al2O3 after zeolite activation, and also a decrease in the amount of impurities. The crystalline phase of the zeolite was carried out using XRD analysis, indicating the type of zeolite used is modernite. The SiO2 phase in the sample is quartz, and the Al2O3 phase is corundum. The average crystal size decreased after activation, from 14.23 nm to 6.85 nm for HCl and 5.42 nm for H2SO4. Futhermore, the surface morphology of all zeolite samples has a form of irregular spherical surface, and the surface size of the particles after activation shows a smaller particle shape. The results of this study are expected to become recommendations for further research related to natural zeolite pretreatment as a catalyst support.
Co-Authors Abd Rahman Abd. Rahman Aulia Rahma Diana Eka Pratiwi Munawwarah Munawwarah Nita Magfirah Ilyas Satria Putra Jaya Sumiati Side Zubair, Sakinah