Molekul: Jurnal Ilmiah Kimia
Vol 13, No 1 (2018)

Surface-enhanced Raman Scattering (SERS) Substrate of Colloidal Ag Nanoparticles Prepared by Laser Ablation for Ascorbic Acid Detection

Teguh Endah Saraswati (Dep of Chemistry, Sebelas Maret University)
Yudha Pratama Putra (LIPI Fisika)
Mohammad Rifqi Ihsan (Unknown)
Isnaeni Isnaeni (Research Center for Physics, Indonesian Institute of Sciences)
Yuliati Herbani (Research Center for Physics, Indonesian Institute of Sciences)



Article Info

Publish Date
31 May 2018

Abstract

Ag nanoparticles were synthesized by laser ablation using an Ag plate in distilled water. This method was performed using a laser with a wavelength of 532 nm and energy of 30 mJ for 60 min. Ag nanoparticles successfully formed, confirmed by the selected area electron diffraction (SAED) which revealed four principal crystal planes of (111), (200), (220) and (311). The size distribution of Ag nanoparticles ranged from 5 to 40 nm, as estimated from electron imaging observed by transmission electron microscope (TEM). Ascorbic acid was used as the analyte to test the characteristics of surface-enhanced Raman scattering (SERS) of colloidal Ag nanoparticles. The concentration of ascorbic acid (1.0, 0.5 and 0.25 wt%) and incubation time (0 and 6 h) were varied to determine the limit of detection and the effect of incubation time. The Raman scattering spectroscopy results showed that the colloidal Ag nanoparticle substrate improved the signals for detection of ascorbic acid.

Copyrights © 2018






Journal Info

Abbrev

jm

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Chemistry

Description

MOLEKUL is a peer-reviewed journal of chemistry published by the Department of Chemistry, Faculty of Mathematics and Natural Sciences, Jenderal Soedirman University, Indonesia. Publishing frequency 2 issues per year, on May and November. This Journal encompasses all branches of chemistry and its ...