Jurnal Kimia (Journal of Chemistry)
Vol.14 No.1 Januari 2020

SINTESIS DAN KARAKTERISASI SILIKA GEL DARI ABU VULKANIK GUNUNG AGUNG MELALUI TEKNIK SOL-GEL

N. P. S. N. Utari (Program Studi Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Udayana)
I W. Sudiarta (Program Studi Kimia FMIPA Universitas Udayana, Jimbaran, Bali, Indonesia)
P. Suarya (Program Studi Kimia FMIPA Universitas Udayana, Jimbaran, Bali, Indonesia)



Article Info

Publish Date
01 Feb 2020

Abstract

Mount Agung in Karangasem, Bali which erupted in September 2017 produced abundant volcanic ash. This ash can be used as a raw material for making silica gel. The stages of the research carried out included analysis of the content of silicon (Si), synthesis of silica gel using sol-gel technique, characterization using FTIR, X-RD instruments as well as surface acidity. The results of the analysis using the X-RD instrument showed the presence of silicon from SiO2 found at 2? = 28,07530. The silica gel yield obtained in this study was 15.05% w/w. The results of the characterization with the FTIR instrument showed that silica gel from volcanic ash of Mount Agung had the main Si-OH and Si-O-Si groups. The hydroxyl bond from Si-OH grup were found at ±3649.32 cm-1 for stretching vibrations and ±1687,71 cm-1 for bending vibrations. Si-O bond from Si-O-Si group were found at ±1207.44 cm-1 for asymmetric stretching vibrations and ±482.20 cm-1 for bending vibrations. Diffractogram showed that the silica gel had an amorphous structure with surface acidity of 18.0222 mmol/g and a surface area of 36.5514 m2/g. Keywords: Agung mountain, silica gel, sol-gel, vulcano ash

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Journal Info

Abbrev

jchem

Publisher

Subject

Chemistry

Description

Jurnal Kimia (Journal of Chemistry) publishes papers on all aspects of fundamental and applied chemistry. The journal is naturally broad in scope, welcomes submissions from across a range of disciplines, and reports both theoretical and experimental ...