Jurnal Kimia (Journal of Chemistry)
Vol. 9, No. 2 Juli 2015

SINTESIS SILIKA GEL TERIMOBILISASI DIFENILKARBAZON DARI ABU SEKAM PADI MELALUI TEKNIK SOL GEL

Ni Nyoman Sri Nopianingsih (Unknown)
I Wayan Sudiarta (Unknown)
Wahyu Dwijani Sulihingtyas (Unknown)



Article Info

Publish Date
01 Jul 2015

Abstract

A research on synthesis diphenylcarbazone immobilized silica gel from rice husk ash by sol-gel technique has been conducted. The purpose of this research was to synthesize the diphenylcarbazone immobilized silica gel from rice husk ash by sol-gel technique.  This research included modification of silica gel of rice husk ash and silica gel characterization by IR spectra and X-RD. The results showed that the diphenylcarbazone immobilized silica gel has been successfully synthesized. It can be seen from the FTIR spectrum that silica-imobilized revealed peaks at wave numbers of ±1087.85cm-1 indicating the presence of Si-O-Si. The peak seen at wave numbers of  ±952.84cm-1 indicating the presence of Si-O, at ±3361.93cm-1due to the Si-OH bond which was the main functional group  of silica gel. Another peaks at ±3313.71cm-1, ±800.46cm-1, ±1602.85cm-1,±1700 cm-1, and ±1602.85cm-1 suggesting the presence of N-H, aromatic C-H (substituted benzene), aromatic C=C, N=N and C=O stretching. X-RD data showed that the structure of diphenilcarbazone immobilized silica gel was amorphous.

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Journal Info

Abbrev

jchem

Publisher

Subject

Chemistry

Description

Jurnal Kimia (Journal of Chemistry) publishes papers on all aspects of fundamental and applied chemistry. The journal is naturally broad in scope, welcomes submissions from across a range of disciplines, and reports both theoretical and experimental ...