YOUNGSTER PHYSICS JOURNAL
Vol 2, No 3 (2013): Youngster Physics Journal Juli 2013

SINTESIS DAN KARAKTERISASI PIGMEN HEMATIT (α-Fe2O3) DARI BIJIH BESI ALAM MELALUI METODE PRESIPITASI

Kukuh Dwi Septiana (Jurusan Fisika, Fakultas Sains dan Matematika, Universitas Diponegoro)
Priyono Priyono (Jurusan Fisika, Fakultas Sains dan Matematika, Universitas Diponegoro)
Nurul Taufiqu Rochman (Pusat Penelitian Metalurgi, Lembaga Ilmu Pengetahuan Indonesia (LIPI) dan Fakultas Teknik, Universitas Teknologi Sumbawa)
Yuswono Yuswono (Pusat Penelitian Metalurgi, Lembaga Ilmu Pengetahuan Indonesia (LIPI))
Tito Prastyo Rahman (Departemen Ilmu Material, Universitas Indonesia)
Dwi Wahyu Nugroho (Departemen Ilmu Material, Universitas Indonesia)
Radyum Ikono (Fakultas Teknik, Universitas Teknologi Sumbawa dan NanoCenter Indonesia)
Nofrizal Nofrizal (Pusat Penelitian Metalurgi, Lembaga Ilmu Pengetahuan Indonesia (LIPI))
Nurwenda Novan Maulana (Fakultas Teknik, Universitas Teknologi Sumbawa dan NanoCenter Indonesia)



Article Info

Publish Date
01 Jul 2013

Abstract

Indonesia has a lot of mining material of iron ore that could be used for various purposes in the steel industry or for pigment manufacturing. This research, has synthesized the Hematite (α-Fe2O3) pigment manufacture through a precipitation mechanism. The iron ore powder is mixed with HCl and NH4OH, then it is dried at a temperature of 150oC and calcinated at a temperature of 500oC and 800oC for knowing the formation temperature of  α-Fe2O3 crystal’s structure. Next, the synthesis results are characterized with XRD at 2θ from 10o to 80o with a sampling pitch of 0,02o. Synthesis results show that the raw material has a lattice parameter values a = b = 5,017 Ǻ and c = 13,652 Ǻ after purifying, the values of lattice parameter become a = b = 5,030 Ǻ and c = 13,739 Ǻ which appropriate with standard of ICDD No. 33-0664. The crystallite size is at range of 40 nm while the lattice strain at 1,700 x 10-4 to 3,500 x 10-4. The results of the color test indicate calcination value L * a * b * = 28,36, 27,86, 30,24 at temperature of 500oC where as at 800oC of the calcination temperature obtain values L * a * b * = 20,47, 22,42, 18,17.Keywords: iron ore, pigments, α-Fe2O3, precipitation

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