Indonesian Journal of Chemical Analysis (IJCA)
Vol. 3 No. 1 (2020): Indonesian Journal of Chemical Analysis

Characterization of Cr/SiO2/Al2O3 catalyst from Rice Husk using Impregnation Method

Prahadu Susmanto (Sriwijaya University)
Yandriani Gusman (Sriwijaya University)
M Fajar Ridwan (Sriwijaya University)
Endra Hakim Tanara (Sriwijaya University)



Article Info

Publish Date
15 Mar 2020

Abstract

Rice husk is one of biomass which has very high silica content (18-22%). It can be used as one of support material in the form of SiO2 / Al2O3 which if it is varied with metals, it will produce a catalyst. In this research, a Cr / SiO2 / Al2O3 catalyst was made by using wetness impregnation and dry impregnation methods to obtain the best amount of Cr metal. According to FTIR test results on SiO2 / Al2O3 material, it formed Si-OH bond (3250.2 cm-1), Al-OH (1620 cm-1), Si-O-Si (1410.6 cm-1), O-Al -O (767.8 cm-1). The results of SEM-EDX and Brunauer Emmet Teller (BET) test on variations in the concentration of 0.5 M precursor solution; 1 M; 1.5 M showed that A3 variant had the highest Cr content of 19.79% with a surface area of 68.939 m2 / gr, a pore volume of 0.06675 cc / gr and a pore radius of 19.36 Å. Based on isothermal desorption adsorption curve with nitrogen gas the A3 catalyst variant was classified into type IV with mesoporous structure based on  International Union of Pure and Applied Chemistry (IUPAC).

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Journal Info

Abbrev

IJCA

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Chemistry Environmental Science

Description

IJCA (Indonesian Journal of Chemical Analysis) is a chemistry journal published by Chemical Analysis Department, Faculty of Mathematics and Natural Sciences, Universitas Islam Indonesia. IJCA publishes original research articles or review articles on aspect all of the chemistry fields especially in ...