Jurnal Sains Materi Indonesia
Vol 21, No 4: JULY 2020

BIOREDUCTION AND CHARACTERIZATION OF SILVER NANOPARTICLES FROM OIL PALM EMPTY FRUIT BUNCH

Siti Suhartati (Academy of Analytical Chemistry Caraka Nusantara, Jl.Tugu Raya Komplek Timah, Depok, 16951)
Iwan Syahjoko Saputra (Unknown)
Dwinna Rahmi (Balai Besar Kimia dan Kemasan, Kementerian Perindustrian RI, Jl. Balai Kimia I Pekayon, Pasar Rebo, Jakarta Timur, 13710)
Yoki Yulizar (Department of Chemistry, FMIPA-UI, Kampus Baru Universitas Indonesia, Depok, 16424)
Sudirman Sudirman (Center for Science and Technology of Advanced Materials-BATAN, Puspitek Area, Serpong, South Tangerang, 15314)



Article Info

Publish Date
15 Dec 2020

Abstract

BIOREDUCTION AND CHARACTERIZATION OF SILVER NANOPARTICLES FROM OIL PALM EMPTY FRUIT BUNCH (OPEFB). The synthesis of silver nanoparticles was successfully carried out by extracting oil palm empty fruit bunch. The precursor used was silver nitrate (AgNO3) with a concentration of 9x10-4 M and 5 wt% of the oil palm empty fruit bunch extract. OPEFB acted as a capping agent in the synthesis of silver nanoparticles. The bioreduction method Ag+ to Ag0 produced a silver nanoparticle colloid in brown color. The results of the UV-Vis spectrophotometer showed the silver nanoparticles colloids spectrum at a wavelength of 420 nm with an absorbance value of 0.5. FTIR shows the reduction and shift of absorption peak in the hydroxyl functional group (-OH) at wavenumbers of 3323 cm-1 and the presence of absorption peaks at 560 cm-1. While, XRD pattern showed the specific crystallinity peaks of silver nanoparticles at 2θ: 33.24°; 39.98°; 61.23°; dan 79.13° respectively with the face-centered cubic crystal structure (FCC) and crystallite size of 15 nm. PSA analysis showed two specific peaks with an average size distribution silver nanoparticles of 43.5 nm and a PDI value of 0.4. Analysis of TEM shows the average particle size of 20 nm with a spherical particle shape.

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Journal Info

Abbrev

jsmi

Publisher

Subject

Materials Science & Nanotechnology

Description

Jurnal Sains Materi Indonesia (Indonesian Journal of Materials Science), diterbitkan oleh Pusat Teknologi Bahan Industri Nuklir - BATAN. Terbit pertama kali: Oktober 1999, frekuensi terbit: empat ...