IJFAC (Indonesian Journal of Fundamental and Applied Chemistry)
Vol 6, No 1 (2021): February 2021

Synthesis and Characterization of Amorphous TiO2 Anode Prepared by Anodizing Method for Na-ion Batteries

Dwi Indrawati (Sriwijaya University)
Nirwan Syarif (Department of Chemistry, Faculty of Mathematic and Natural Sciences, Sriwijaya University)
Dedi Rohendi (Department of Chemistry, Faculty of Mathematic and Natural Sciences, Sriwijaya University)



Article Info

Publish Date
20 Feb 2021

Abstract

Sodium ion battery (SIB) has engage sustainable alternative on replacing lithium ion batteries. The lower potential and larger ionic value has demanded on seeking a potential anode materials. Amorphous TiO2 prepared by electrochemical anodisation technique has provide a suitablility as anode SIB materials, which approved by conducting XRD, FTIR, and SEM-EDX measurements. Electrochemical performance was tested with variations in the concentration of NaOCl4 electrolyte in propylene carbonate (PC) solvent. Diffractogram of TiO2 showed the only peaks of Ti was observed at 2θ = 40.34. The TiO2 IR spectrogram shows that the absorption band at 507 cm-1 is the peak of the vibration characteristics of the Ti-O bond and the peak of 975 cm-1 corresponds to Ti-O-Ti bond. SEM-EDX image analysis showed the morphology of TiO2 was smooth without pore with a ratio of Ti: O elemental composition of 1: 2. Voltammogram showed the anodes in 0.5 M NaOCl4 electrolyte in PC solvent has a good stability potential windows with the high current density 1.2 mA and the capacity of 0.037 F/g

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Journal Info

Abbrev

IJFAC

Publisher

Subject

Biochemistry, Genetics & Molecular Biology Chemistry Environmental Science

Description

Indonesian Journal of Fundamental and Applied Chemistry (IJFAC) is an international research journal and invites contributions of original research articles as well as review articles in several areas of chemistry. The journal aims to publish refereed, high-quality research papers with significant ...