VALENSI
Jurnal Kimia VALENSI Volume 6, No. 2, November 2020

Facile Chemical Processing of Geloina coaxans Shell and Sodium dihydrogen Phosphate as Precursors to Produce Hydroxyapatite

Pepi Helza Yanti (Chemistry Department, Faculty of Mathematics and Natural Science, Universitas Riau Pekanbaru 28293)
Resti Resmalina (Chemistry Department, Faculty of Mathematics and Natural Science, Universitas Riau Pekanbaru 28293)



Article Info

Publish Date
17 Feb 2021

Abstract

This paper reports the synthesis of hydroxyapatite from Geloina coaxans shell and sodium dihydrogen phosphate as precursors by facile and simple method. Firstly, Geloina coaxans shell calcined at 1000 oC for 12 hours to produce lime or CaO. The chemical composition of Geloina coaxans shell calcined was analyzed using the XRF technique, and the result shows that the main component of Geloina coaxans shell calcined was calcium. Synthesis of hydroxyapatite has been done with stirring and aging time parameters and molar ratio of precursors was 1.67.  The XRD patterns showed a specific peak of hydroxyapatite that appeared at 2θ=31.8 o and based on the XRD results on the aging time indicated that the rate of growth of HAp crystals was better and faster at aging for 12 hours. The crystal size of HAp obtained was 37 nm. The FTIR spectra of hydroxyapatite showed characteristics of hydroxyl and phosphate bands in sample spectra. The morphology of hydroxyapatite synthesized also was examined by SEM and the results showed spherical morphology.

Copyrights © 2020






Journal Info

Abbrev

valensi

Publisher

Subject

Chemistry

Description

Jurnal Kimia Valensi is a biannual and peer-reviewed open access journal published by Department of Chemistry, Faculty of Science and Technology UIN Syarif Hidayatullah Jakarta. This journal covering all aspect of ...