JURNAL KIMIA SAINS DAN APLIKASI
Vol 24, No 5 (2021): Volume 24 Issue 5 Year 2021

Development of a Fast Simultaneous Analysis Method for Determination of Middle Rare-Earth Elements in Monazite Samples

Heru Agung Saputra (Department of Chemistry, Universitas Padjadjaran, Jatinangor, Sumedang 45363|Universitas Padjadjaran|Indonesia)
Anni Anggraeni (Department of Chemistry, Universitas Padjadjaran, Jatinangor, Sumedang 45363|Universitas Padjadjaran|Indonesia)
Abdul Mutalib (Department of Chemistry, Universitas Padjadjaran, Jatinangor, Sumedang 45363|Universitas Padjadjaran|Indonesia)
Husein Hernandi Bahti (Department of Chemistry, Universitas Padjadjaran, Jatinangor, Sumedang 45363|Universitas Padjadjaran|Indonesia)



Article Info

Publish Date
31 Jul 2021

Abstract

Rare earth elements are a set of seventeen metallic elements, which is an essential part of many high-tech devices. Hence, analysis and/or separation of the rare earth elements from their mineral become crucial. A novel analysis method combining ultraviolet-visible spectroscopic and multivariate analysis was developed to determine middle rare earth elements quickly and simultaneously. The data collected from ultraviolet-visible spectroscopic were analyzed by multivariate analysis. The results showed that the developed method has good accuracy and precision with a detection limit of 1.375 (± 0.012), 0.332 (± 0.004), 42.117 (± 0.200), 1.767 (± 0.011), and 0.576 (± 0.002) ppm, respectively for samarium, europium, gadolinium, terbium, and dysprosium. The interference effect of ammonium iron(II) sulfate hexahydrate, manganese(III) sulfate hydrate, calcium carbonate, sodium carbonate, and lead(II) nitrate were examined. The reliability of the proposed method was evaluated using monazite samples. Conclusively, the developed method was successfully applied to determine the middle rare earth elements in monazite samples.

Copyrights © 2021






Journal Info

Abbrev

ksa

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Chemistry Engineering

Description

urnal Kimia Sains dan Aplikasi (p-ISSN: 1410-8917) and e-ISSN: 2597-9914) is published by Department of Chemistry, Diponegoro University. This journal is published four times per year and publishes research, review and short communication in field of ...