Mechatronics, Electrical Power, and Vehicular Technology
Vol 13, No 1 (2022)

Carbon electrode sensitivity enhancement for lead detection using polypyrrole, ionic liquid, and nafion composite

Zanu Saputra (Politeknik Manufaktur Negeri Bangka Belitung)
Robeth Viktoria Manurung (Research Center for Telecommunication, National Research and Innovation Agency (BRIN))
Aminuddin Debataraja (Politeknik Negeri Jakarta)
Muhammad Iqbal Nugraha (Politeknik Manufaktur Negeri Bangka Belitung)
Tien-Fu Lu (The University of Adelaide)



Article Info

Publish Date
29 Jul 2022

Abstract

This paper concerns enhancing a lead detection sensor using a combination of polypyrrole (PPy), Nafion (N), and ionic liquid (IL) with thick-film or screen-printing technology on sensitive material-based carbon electrodes. Electrode characterization using a scanning electron microscope (SEM) was conducted to see the morphology of sensitive materials, showing that the spherical particles were distributed evenly on the electrode surface. Analysis using energy dispersive spectroscopy (EDS) shows that the element's atomic composition is 84.92 %, 8.81 %, 6.26 %, and 0.01 % for carbon, nitrogen, oxygen, and bismuth, respectively. Potentiostat measurement with the ambient temperature of 25 °C on a standard lead solution with concentration ranging from 0.05 to 0.5 mg/l yields an average output voltage ranging from 2.16 to 2.27 V. It can be concluded that the sensor is able to detect lead with a sensitivity of 0.21 V in each addition of solution concentration (mg/l) and give an 84 % concentration contribution to the voltage.

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Journal Info

Abbrev

mev

Publisher

Subject

Electrical & Electronics Engineering

Description

Mechatronics, Electrical Power, and Vehicular Technology (hence MEV) is a journal aims to be a leading peer-reviewed platform and an authoritative source of information. We publish original research papers, review articles and case studies focused on mechatronics, electrical power, and vehicular ...