Makara Journal of Technology
Vol. 21, No. 1

Nano-Channels Early Formation Investigation on Stainless Steel 316Ti after Immersion in Molten Pb-Bi

Rivai, Abu Khalid (Unknown)
Mardiyanto, Mardiyanto (Unknown)
Heinzel, Annette (Unknown)



Article Info

Publish Date
01 Apr 2017

Abstract

Development of fuel cladding and structural materials in Pb-Bi environment, especially at high temperature, is a critical issue for the deployment of LFR (Lead alloy-cooled Fast Reactor) and ADS (Accelerator Driven Transmutation System). This is because of the corrosive characteristic of Pb-Bi to metals as constituent materials of fuel cladding and structural of the reactors. Corrosion test of a high-chromium austenitic stainless steel i.e. SS316Ti in molten Pb-Bi at 550 ÂșC has been carried out for about 300 hours continuously. The characterization using SEM-EDS (Scanning Electron Microscopy - Energy Dispersive X-ray Spectroscopy) showed that an iron oxide as the outer layer and a chromium oxide as the inner layer on the surface of the specimen were formed which in general have protected the steel specimen from corrosion and dissolution attack of Pb-Bi. However, small amount of Pb could penetrate into the iron oxide layer through ultra-narrow channels. Atomic Force Microscopy (AFM) with Electrostatic Force Microscopy (EFM) mode was employed to investigate the phenomena of the nano-channels early formation. The results of the nano-scale investigation showed clearly the formation of the channels at the early time of corrosion as the way of Pb to penetrate into iron oxide outer layer.

Copyrights © 2017






Journal Info

Abbrev

publication:mjt

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Civil Engineering, Building, Construction & Architecture Electrical & Electronics Engineering Engineering Materials Science & Nanotechnology Mechanical Engineering

Description

MAKARA Journal of Technology is a peer-reviewed multidisciplinary journal committed to the advancement of scholarly knowledge and research findings of the several branches of Engineering and Technology. The Journal publishes new results, original articles, reviews, and research notes whose content ...