Makara Journal of Science
Vol. 7, No. 1

PREPARATION of [BzMe3N]2[Na2W4O12(OMe)4(MeOH)6].6MeOH

Bakri, Ridla (Unknown)



Article Info

Publish Date
25 Apr 2003

Abstract

An attempt to prepare trinuclear tungsten oxoalkoxides [BzMe3N]3 [W3O8 (OMe)5 ] from the reaction between WO2 (OMe)2 , [BzMe3N]2WO4 and [BzMe3N](OMe) in the ratio of 2:1:1 in MeOH produced [BzMe3N]2 [Na2W4O12(OMe)4 (MeOH)6 ].6MeOH. Suitable crystals for X-ray chrystallographic studies were obtained from hot mixture of methanol-acetonitrile solution. The I.R., 1H-NMR, and microanalysis data including crystal structure of [Na2W4O12(OMe)4 (MeOH)6 ] 2- anion are reported

Copyrights © 2003






Journal Info

Abbrev

publication:science

Publisher

Subject

Description

Makara Journal of Science publishes original research or theoretical papers, notes, and minireviews on new knowledge and research or research applications on current issues in basic sciences, namely: Material Sciences (including: physics, biology, and chemistry); Biochemistry, Genetics, and ...