TEKNIK
Vol. 44, No. 2 (2023): August 2023

Mg-0.5Ca-4Zn-xCaCO3 (x=8, 10) Alloy Foams with Closed-Pore Structure Synthesized by Powder Metallurgy Process for Implant Applications

Aprilia Erryani (National Research and Innovation Agency)
Franciska Pramuji Lestari (National Research and Innovation Agency)
Joko Triwardono (National Research and Innovation Agency)
Bunga Rani Elvira (National Research and Innovation Agency)
Bintoro Siswayanti (National Research and Innovation Agency)
Albertus Deny Hadi Setiawan (National Research and Innovation Agency)



Article Info

Publish Date
30 Aug 2023

Abstract

This work aims to synthesize Mg-0.5Ca-4Zn alloy foams using a CaCO3 foaming agent and a powder metallurgy (PM) process. Mg-0.5Ca-4Zn-xCaCO3 (x=8, 10 wt.%) alloy precursors were prepared by mixing Mg, Ca, and Zn metal powders with CaCO3 granules, compacting, and then sintering at various temperatures (i.e., 650, 675, and 700 °C) for 5 hours in an argon atmosphere. The pore morphology was observed by scanning electron microscopy (SEM), and the phase formation was analyzed using X-ray diffractometry (XRD). The density and porosity were evaluated using an Archimedes test (ASTM B311-93). The compressive strength was examined using a universal testing machine (UTM) with a constant crosshead speed of 1.3 mm/min (ASTM D695-02). SEM observation reveals the formation of pores with a closed-cell type structure in all alloy compositions. Increasing either the CaCO3 content or sintering temperature results in an increase in porosity and pore sizes but a decrease in compressive strength. The maximum porosity of 43.208% was obtained in the alloy foam with 10 wt.% CaCO3 sintered at 700 °C; the foam exhibits a compressive strength of 52.9 MPa, close to cancellous bone.

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Journal Info

Abbrev

teknik

Publisher

Subject

Engineering

Description

Journal yang mempublikasikan artikel-artikel ilmiah dari berbagai disiplin ilmu rekayasa/keteknikan. Artikel-artikel yang dipublikasikan di Jurnal TEKNIK meliputi hasil-hasil penelitian ilmiah asli (prioritas utama), artikel ulasan ilmiah yang bersifat baru (tidak prioritas), atau komentar atau ...