BRIDGE: The Multidisciplinary Research Portal
Vol. 1 No. 1 (2023): BRIDGE: The Multidisciplinary Research Portal

The Influence of Lampung Natural Lime Temperature and Heating Time on The Physical Properties and Hardness of Hydroxy Products (HA)

Agus Hendriyanto (Sekolah Tinggi Teknologi Nusantara Lampung)



Article Info

Publish Date
14 Aug 2023

Abstract

Hydroxyapatite (HA), a vital component for tissue and porous applications, holds promise in bone regeneration. Derived from calcium carbonate (CaCO3), it's essential for biocompatibility in human bone replacement. This study aims to harness Lampung Province's limestone as a raw material for HA synthesis, simulating human bone properties. Ball milling (2, 3, and 4 hours at 300 rpm) and sintering (600 °C, 800 °C, and 1000 °C for 2, 3, and 4 hours) were varied, with analyses encompassing FTIR, XRD, SEM-EDX, and Vickers hardness. Mountain branch limestone, comprising 97.43% CaCO3, serves as a suitable bone substitute. FTIR spectra of calcined lime powder exhibit PO43-peaks at 1025.45 cm1, Ca-O vibrations at 1413.59 cm1, and OH groups at 3030.33 cm1, mimicking commercial HA. XRD patterns closely resemble the commercial product, with a peak at 2 32.26°. SEM-EDX analysis at 1000 °C for 4 hours reveals a uniform microstructure. Among milling processes, 2-hour milling at 300 rpm exhibits the highest calcium and phosphate levels in EDX results. Vibration testing indicates peak hardness at 1000 °C and 4 hours of processing.

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Journal Info

Abbrev

bridge

Publisher

Subject

Engineering

Description

BRIDGE The Multidisciplinary Research Portal is an open access academic journal that publishes multidisciplinary research articles in various fields, including science and technology, health, social and humanities, arts and humanities, business and economics, and education. The journal aims to ...