Jurnal Teknik Mesin
Vol 16 No 2 (2023): Jurnal Teknik Mesin

Optimalisasi Temperatur Sintering Pada Sintered Body Hidroksiapatit Dengan Penambahan Silika Sebagai Material Penguat

Erdinal - Febri (Teknik Mesin, Fakultas Teknik, Institut Teknologi Padang)
Azisyam Pajri (Teknik Mesin, Fakultas Teknik, Institut Teknologi Padang)
Ade Indra (Teknik Mesin, Fakultas Teknik, Institut Teknologi Padang)



Article Info

Publish Date
01 Dec 2023

Abstract

Sintered body hydroxyapatite (HA) in the form of pellets has been made by adding silica as a reinforcing material (ratio 60:40 wt.%) by varying the sintering temperature. HA and silica were subjected to a dry mixing process for 2 h, then a wet mixing process was carried out for 2 h with the addition of PVA and alcohol as a binder. The mixing process uses a rotary drum with the addition of zirconia balls with the aim of making the mixture more homogeneous. After the mixing process, the samples were dried for 48 h to remove the alcohol contained. The green body was made using the uniaxial pressing method at a pressure of 100 MPa and held for 3 minutes. The sintering process is carried out variously at temperatures of 800°C, 900°C, 1000°C, 1100°C, 1200°C, 1300°C, and 1400°C. with a heating rate of 5ºC/minute and holding time of 4 h. Next, the temperature was lowered to 300ºC with a cooling rate of 5ºC/minute. The results showed that linear shrinkage increased significantly (weight shrinkage increased 12.83% - 25.08% and diameter shrinkage increased 3.26% - 23.21%). The results of the relative density calculation show that there is a significant increase with each variation in sintering temperature, where the increase occurs from 44.4% - 85.6%. The compressive strength value also shows an increase with increasing sintering temperature, namely from 21.2 MPa at 800 oC to 65.9 MPa at 1300 oC. Meanwhile, at a sintering temperature of 1400°C, compressive strength values decreased and oxidation occurred as evidenced by color changes. It can be concluded that the optimization of the sintering process occurs at a temperature of 1300 oC which is proven by the highest compressive strength value and no oxidation occurs.

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Journal Info

Abbrev

jtm

Publisher

Subject

Automotive Engineering Energy Engineering Materials Science & Nanotechnology Mechanical Engineering

Description

Jurnal Teknik Mesin adalah sebuah jurnal peer review yang didedikasikan untuk publikasi hasil penelitian yang berkualitas dalam bidang teknik mesin. ...