Jurnal Fisika Unand
Vol 13 No 6 (2024)

Studi Pendahuluan Uji Aktivitas Katalitik Katalis Montmorillonit K-10 Yang Dimodifikasi Cu2+

Admi Admi (Departemen Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Andalas)
Delvi Isnaini (Departemen Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Andalas)
Syukri Syukri (Departemen Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Andalas)



Article Info

Publish Date
22 Nov 2024

Abstract

The current study examines the catalytic activity of Cu2+-exchanged cation montmorillonite K-10 (MMT K-10) catalyst, which synthesized by hydrothermal method. X-ray fluoressence (XRF) and X-ray Diffraction (XRD) were used for characterizing the newly synthesis catalyst. The effect of thermal activation on the support of MMT K-10 with a modifier Cu investigated on its catalytic performance for conversion waste cooking oil to produce fatty acid methyl ester (FAME) by transesterification reaction. Synthesis biodiesel was further characterized by Gas Chromatography-Mass Spectroscopy (GC-MS). The biodiesel was obtained at transesterification reaction conditions: 3% (w/w) catalyst loading, molar ratio of oil to methanol = 1:10, and 3 h of reaction time at 90°C. The yield of FAME of WCO for MMT K-10, MMT K-10/Cu2+, MMT K-10 (activation 110°C)/Cu2+, MMT K-10 (activation 300°C)/Cu2+ catalysts were the 9,47%; 10,36%; 10,41%; and 12,01% of FAME, respectively. This study exhibites that the activation of thermal on the support MMT K-10 which modified by Cu2+ leads to reduction of the crystal size. The decreasing crystal size contributes on increasing catalytic performance of the heterogeneous catalyst.

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Journal Info

Abbrev

jfu

Publisher

Subject

Earth & Planetary Sciences Electrical & Electronics Engineering Energy Materials Science & Nanotechnology Physics

Description

Makalah yang dapat dipublikasikan dalam jurnal ini adalah makalah dalam bidang Fisika meliputi Fisika Atmosfir, Fisika Bumi, Fisika Intrumentasi, Fisika Material, Fisika Nuklir, Fisika Radiasi, Fisika Komputasi, Fisika Teori, Biofisika, ataupun bidang lain yang masih ada kaitannya dengan ilmu ...