ALCHEMY Jurnal Penelitian Kimia
Vol 20, No 2 (2024): September

Microwave-Assisted Synthesis of Corn Husk-Based Hydrogels Grafted with Acrylamide

Ginanjar Penata Aji (Universitas Sebelas Maret Jalan Ir. Sutami 36 A, Kentingan, Surakarta, Central Java, 57126, Indonesia)
Mahira Noor Syevarani Arifandi (Universitas Sebelas Maret Jalan Ir. Sutami 36 A, Kentingan, Surakarta, Central Java, 57126, Indonesia)
Sperisa Distantina (Universitas Sebelas Maret Jalan Ir. Sutami 36 A, Kentingan, Surakarta, Central Java, 57126, Indonesia)
Mujtahid Kaavessina (Universitas Sebelas Maret Jalan Ir. Sutami 36 A, Kentingan, Surakarta, Central Java, 57126, Indonesia)



Article Info

Publish Date
30 Sep 2024

Abstract

Corn husk waste contains cellulose, which has the potential as a raw material for hydrogel preparation. Hydrogels can be applied as water purification, diapers, and superabsorbents. This study aimed to synthesize hydrogel from corn husk cellulose grafted with acrylamide monomer using a microwave-assisted grafting method. Potassium peroxodisulfate (PPD) was used as an initiator, and the effects of acrylamide and PPD on hydrogel swelling capacity were investigated. The process involved drying and crushing corn husks into powder, then mixing the powder with acrylamide and PPD for microwave grafting to form a polymer, which was then ground into powder. The grafted polymer was combined with carrageenan to create bead gels soaked in distilled water and urea to measure swelling capacity. Results showed that swelling capacity increased with more acrylamide and decreased with more PPD. The highest swelling capacity reached 1016.16% in water and 961.6% in urea. FTIR analysis confirmed the successful grafting of acrylamide onto corn husk cellulose by detecting changes in the infrared spectrum. Based on FTIR and swelling capacity data, it was concluded that the grafting process was completed using the microwave method with PPD as the initiator.

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Journal Info

Abbrev

alchemy

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Chemistry Energy Environmental Science Materials Science & Nanotechnology

Description

ALCHEMY Jurnal Penelitian Kimia is a chemistry journal published by Sebelas Maret University, Surakarta. ALCHEMY Jurnal Penelitian Kimia publishes original research articles or review articles in organic chemistry, inorganic chemistry, analytical chemistry, physical chemistry, biochemistry, and ...