UPAYA ISOLASI β-ASARONE PADA EKSTRAK n-HEKSAN RIMPANG DRINGO (Acorus calamus L.) ASAL KABUPATEN PINRANG

Siti Sya'diyah (Fakultas Farmasi Universitas Muslim Indonesia)
Risda Waris (Fakultas Farmasi Universitas Muslim Indonesia)
Ahmad Najib (Fakultas Farmasi Universitas Muslim Indonesia)

Jurnal Fitofarmaka Indonesia
Vol 1, No 1 (2014): JURNAL FITOFARMAKA INDONESIA

The isolation of n-hexane extract from Sweet Flag rhizome (Acorus calamus L.) was done. The aim of this research is to obtain β-asarone isolate as marker compound of   Sweet Flag (Acorus calamus L.). Sample from 1 kg of dried rizhome, mascerate using n-hexane. This process produce 31 ml thick extract. Isolation of n-hexane extract using column chromatography with isocratic methode using n-hexane etil acetat 8 : 2.  The isolate identified by UV-Vis spectroscopy,  IR spectroscopy,  (1H) NMR and Gas Chromatography Mass Spectro. From the data result show that isolate is β-asarone.