<![CDATA[The research aimed to optimize the quality attributes of Piper retrofractum Vahl.—piperine content, color brightness, and water content—using Partial Least Squares Regression (PLSR) to evaluate the pretreatment effects with fruit peel infusions and drying conditions. The research urgency lied in addressing the challenges of achieving consistent product quality while promoting sustainable food processing practices. Around 30 samples of Piper retrofractum Vahl. were subjected to varying pretreatment concentrations, soaking durations, drying durations, and peel types (orange and pineapple). The PLSR model was employed to identify key factors influencing the quality attributes and assess predictive performance based on Root Mean Squared Error (RMSE) and Coefficient of Determination (R²) values. As a result, the PLSR model explains 43.22% of the variance in piperine content, highlighting the importance of shorter soaking durations and higher pretreatment concentrations in preserving piperine levels. For water content, the model captures 75.08% of the variance, emphasizing the critical role of drying duration in reducing moisture. However, the color brightness model explains only 18.5% of the variance, indicating the need to explore contributing factors further. The research introduces the innovative use of fruit peel-infused water as a sustainable pretreatment method, contributing to eco-friendly food processing practices and offering practical insights into optimizing production for improved product quality. The findings underscore the importance of balancing pretreatment and drying parameters to address inconsistencies in quality while promoting sustainability. Future research should expand experimental conditions, integrate additional variables, and explore advanced modeling techniques to enhance predictive accuracy and product quality.]]>
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