Jurnal Teknologi dan Mutu Pangan
Vol. 2 No. 1 (2023): JTMP: Jurnal Teknologi dan Mutu Pangan

Pengujian Kadar Pengawet Asam Benzoat dan Asam Sorbat Pada Permen Keras Menggunakan Kromatografi Cair Kinerja Tinggi: Determination of Benzoic Acid And Sorbic Acid Preservative Levels In Hard Candies Using High-Performance Liquid Chromatography

Samara, Reizza Muhammad Giyats Al Hisyam Dwi (Unknown)
Yuningsih, Nuning (Unknown)
Putri, Nezly Nurlia (Unknown)



Article Info

Publish Date
31 Jul 2023

Abstract

Hard candy is a solid snack made from sugar or other sweeteners,  sometimes with added food ingredients and food additives (BTP). According to BPOM Regulation No. 11 of 2019, the maximum allowable levels of benzoic acid and sorbic acid in hard candy are 500 mg/kg and 1000 mg/kg body weight. Excessive consumption of these acids can pose health risks. Food quality control of the use of BTP can be done by routine testing in the laboratory. One of the instruments that can detect BTP is High-Performance Liquid Chromatography (HPLC).  This study aims to analyze the levels of benzoic acid and sorbic acid in hard candy samples using an HPLC. The results showed that neither benzoic acid nor sorbic acid was detected in the samples. The LOD value of benzoic acid obtained on the HPLC instrument was 4.92 mg/kg, and the LOD of sorbic acid was 3.70 mg/kg) which limits its use to meet BPOM regulation No. 11 of 2019. The testing process for benzoic acid and sorbic acid in hard candy samples is also correct and by the procedure, where the recovery value is in the range of 90-107%, the RPD value is smaller than the 2/3 CV Horwitz value (In benzoic acid, the RPD value is 1.02% and the CV Horwitz value is 6.42 while in sorbic acid the RPD value is 0.75% and the CV Horwitz value is 4.15) with a correlation coefficient that meets the linearity (r) requirement of 0.9999.

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Journal Info

Abbrev

jtmp

Publisher

Subject

Agriculture, Biological Sciences & Forestry

Description

JTMP-Jurnal Teknologi dan Mutu Pangan merupakan wadah bagi akademisi, peneliti dan praktisi untuk mempublikasikan hasil karya orisinil yang belum pernah diterbitkan sebelumnya. Adapun fokus dan ruang lingkup topik yang diterbitkan pada jurnal ini meliputi: Ilmu pangan; Teknologi pangan; Mikrobiologi ...