Rekayasa Mesin
Vol. 16 No. 2 (2025)

FOURIER TRANSFORM INFRARED SPECTROSCOPY INTERPRETATION DAN THERMOGRAVIMETRY/DIFFERENTIAL SCANNING CALORIMETRY ANALYSIS ON THERMOSETTING RESIN PRODUCTS WITH QUENCHING TREATMENT

Sukanto, Heru (Unknown)
Widodo, Purwadi Joko (Unknown)
Arifin, Zainal (Unknown)
Triyono, Joko (Unknown)



Article Info

Publish Date
15 Aug 2025

Abstract

The quenching phenomenon observed in thermosetting epoxy resins necessitates a comprehensive investigation to mitigate its potential adverse effects on material performance. This study presents a novel approach to analyzing epoxy resins by employing Fourier Transform Infrared (FTIR) spectroscopy, Thermogravimetric Analysis (TGA), and Differential Scanning Calorimetry (DSC). Epoxy resin specimens were fabricated using a 1:1 weight ratio of diglycidyl ether bisphenol A resin and cycloaliphatic amine hardener. The quenching process was executed by submerging the specimens in water at ambient temperature following thermal exposure at 75, 100, 125, and 150°C. The FTIR and TGA/DSC analyses were verified by tensile testing, which revealed that FTIR analysis provided insights into the degree of crosslinking and hydroxyl index, while TGA/DSC data elucidated the glass transition temperature and crosslinking enthalpy. The findings demonstrated a direct correlation between the tensile strength and strain of the epoxy resin with changes in crosslinking enthalpy, and an inverse relationship with the hydroxyl index.

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Journal Info

Abbrev

rm

Publisher

Subject

Mechanical Engineering

Description

Rekayasa Mesin is published by Mechanical Engineering Department, Faculty of Engineering, Brawijaya, Malang-East Java-Indonesia. Rekayasa Mesin is an open-access peer reviewed journal that mediates the dissemination of academicians, researchers, and practitioners in mechanical engineering. Rekayasa ...