Analit: Analytical And Environmental Chemistry
Vol. 9, No. 01 April (2024) Analit : Analytical and Environmental Chemistry

ANALYSIS OF THE EFFECT OF AGING TIME ON AMORPHOUS PHASE NANOSILICA FROM PARANGLOE IGNEOUS ROCKS USING THE SOL-GEL METHOD

Rismawati, Rismawati (Unknown)
Majid, Ahmad Fudhail (Unknown)
Putri, Suriati Eka (Unknown)



Article Info

Publish Date
30 Apr 2024

Abstract

In this research, an analysis of the effect of aging time on amorphous phase nanosilica from Parangloeigneous rock was conducted using the sol-gel method. The research samples were taken from aroundthe Parangloe waterfall in Gowa regency, South Sulawesi province. The research stages includedsample preparation, nanosilica synthesis using the sol-gel method, and synthesis resultscharacterization. Characterization was performed using XRF, XRD, SEM-EDX, and PSA. XRF datashowed that the silica content was 53.62% in the form of white powder, and after synthesis, itdecreased to 12.38%. SEM-EDX testing results showed small agglomerated spheres with an EDX of4.52%. A 3-hour aging time variation resulted in an amorphous phase, making 3 hours the optimumtime for amorphous phase nanosilica formation with the highest peak intensity at 2θ=25.42 ° and aparticle size of 170.8 nm.  

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Journal Info

Abbrev

analit

Publisher

Subject

Chemistry Energy Environmental Science

Description

Analit is a scientific journal that contains research results and reviews in the field of analytics and the environment. Fields of research studies or review articles that can be published in this journal include analytical chemistry, biosensor, chemical sensor, synthesis and characterization of ...