The Journal of Pure and Applied Chemistry Research
Vol. 14 No. 3 (2025): Edition September-December 2025

Synthesis and Characterization Composite Fe3O4/Chitosan-PVA/TiO2 for Photocatalytic Degradation of Tetracycline

Denada, Laellia (Unknown)
Poedji Loekitowati Hariani (Unknown)
Addy Rachmat (Unknown)



Article Info

Publish Date
26 Nov 2025

Abstract

This research aims to synthesize tetracycline waste which pollutes the environment, can be overcome by a photocatalytic degradation process using a Fe3O4/Chitosan-PVA/TiO2 composite synthesized using the coprecipitation method. The Fe3O4/Chitosan-PVA/TiO2 composite was characterized by X-Ray Diffraction (XRD), Scanning Electron Microscope- Energy Dispersive Spectroscopy (SEM-EDS), Vibrating Sample Magnetometer (VSM), Ultraviolet-Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS) and pHpzc. The crystallite size of 28.29 nm. The morphology of the composite shows a heterogeneous form with the constituent elements being C (7.69%), N (12.78), O (14.88%), Fe (63.33%) and Ti (1.29%). The saturation magnetization value of 64.24 emu/g is superparamagnetic with a band gap value of 1.38 eV and pHpzc at pH 6.8. The degradation process was studied by investigating the influence of several parameters, namely, solution pH, tetracycline concentration and irradiation time. The efficiency of tetracycline degradation by Fe3O4/Chitosan-PVA/TiO2 was 94.85% at pH 2, concentration of 15 mg/L and radiation time of 70 minutes. The results of Total Organic Carbon (TOC) analysis in a 15 mg/L tetracycline solution before degradation were 20.3 mg/L and after degradation were 5.59 mg/L with a percent reduction in carbon content of 72.46%.

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Journal Info

Abbrev

jpacr

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Chemistry Materials Science & Nanotechnology Medicine & Pharmacology

Description

The Journal of Pure and Applied Chemistry Research focuses in publishing research articles in the field of Chemistry and Applied Chemistry. The target is in exploring, investigating, and developing chemicals sources from local and/or Indonesian to increase the value. Scope of the journal is organic ...