African Journal of Sciences and Traditional Medicine
Vol 1 No 1 (2024): African Journal of Sciences and Traditional Medicine

Synthesis and Characterisation of Calcined Zeolite X and Silica-Supported Zeolite Y

Abakpa A. M (Unknown)
Leke L (Unknown)
Twan S. M (Unknown)
Japhet T (Unknown)
Ewenifa O. J (Unknown)
Omale, O. P (Unknown)



Article Info

Publish Date
29 Jul 2024

Abstract

Zeolite X was synthesised from rice husk silica and aluminium metal as raw materials while Zeolite Y supported catalyst was synthesised from sodium hydroxide, sodium silicate and alumina as chemical raw materials and was impregnated with rice husk silica by wet impregnation method, the catalyst were subsequently calcined at 550 0C for 6h the catalysts were characterised using XRD, FTIR and SEM. The formation of AlO4/SiO4 catalyst was confirmed by the analysis aforementioned. The XRD revealed that Zeolite X and Y synthesized has a faujasite phase with major peaks 230, 22.50 and 17.50, 180 in zeolite X and Y respectively, SEM confirmed the composition of crystallite shapes of irregular, cubic and rectangular shape. FTIR analyses revealed the presence of functional groups (The signal at the silica-alumina vibrational regions (1300 – 300 cm-1) indicates that SiO4 or AlO4 are linked) associated with Zeolites.

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Journal Info

Abbrev

AJSTM

Publisher

Subject

Chemistry Health Professions Immunology & microbiology Nursing Public Health

Description

African Journal of Sciences and Traditional Medicine aims to publish rigorous, peer-reviewed research that advances scientific knowledge in natural and life sciences while promoting analytically grounded and evidence-informed scholarship in traditional medicine and related biological fields. • ...