Dental Journal (Majalah Kedokteran Gigi)
Vol. 59 No. 3 (2026): September

Synthesis and characterization of beta-tricalcium phosphate /polyacrylic acid composite membrane

Juan Cassius Halim (Undergraduate Student, Faculty of Dentistry, Universitas Trisakti, Jakarta)
Eddy (Department of Dental Material, Faculty of Dentistry, Universitas Trisakti, Jakarta)
Tansza Setiana Putri (Department of Dental Material, Faculty of Dentistry, Universitas Trisakti, Jakarta)
Deviyanti Pratiwi (Department of Dental Material, Faculty of Dentistry, Universitas Trisakti, Jakarta)
Florencia Livia (Department of Dental Material, Faculty of Dentistry, Universitas Trisakti, Jakarta)
Abida Zhafira Inayasary (Department of Dental Material, Faculty of Dentistry, Universitas Trisakti, Jakarta)



Article Info

Publish Date
01 Sep 2026

Abstract

Background: Untreated bone loss can lead to serious complications. Guided Bone Regeneration (GBR) is a promising approach for treating periodontal tissue and alveolar bone defects, in which membranes serve as protective barriers for bone grafts. Purpose: This study aimed to fabricate and characterize a novel membrane composed of β-tricalcium phosphate (β-TCP) and polyacrylic acid (PAA) for potential GBR applications. Methods: β-TCP powder was synthesized using a Ca/P ratio of 1.5 from calcium carbonate and dibasic calcium phosphate dihydrate, followed by ball milling and sintering. The β-TCP membrane was then fabricated by combining β-TCP with PAA at various concentrations. The fabricated membranes were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier-transform infrared spectroscopy (FTIR). Results: XRD analysis confirmed the presence and stability of the crystalline β-TCP structure within the membrane. SEM revealed closely packed β-TCP particles with strong interparticle bonding. FTIR analysis demonstrated chemical interactions between the carboxyl (-COOH) groups of PAA and calcium ions (Ca²⁺) from β-TCP, indicating successful integration of the two components. Conclusion: The β-TCP/PAA membrane exhibited promising structural and chemical properties, supporting its potential as a novel GBR membrane for periodontal tissue regeneration.

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Journal Info

Abbrev

MKG

Publisher

Subject

Dentistry

Description

The Dental Journal (Majalah Kedokteran Gigi) (e-ISSN:2442-9740; p-ISSN:1978-3728) is published by the Faculty of Dental Medicine, Universitas Airlangga. Its diciplinary focus is dental science and dental hygiene. The Dental Journal (Majalah Kedokteran Gigi) is published in English on a quarterly ...