Dental Journal (Majalah Kedokteran Gigi)
Vol. 59 No. 3 (2026): September

Characterization of limestone-based beta-tricalcium phosphate /polyacrylic acid blocks as bone graft candidates

Dianayu Noviani Soesianto Putri (Undergraduate Program, Faculty of Dentistry, Universitas Trisakti, Jakarta)
Tansza Setiana Putri (Department of Dental Materials, Faculty of Dentistry, Universitas Trisakti, Jakarta)
Abida Zhafira Inayasary (Department of Dental Materials, Faculty of Dentistry, Universitas Trisakti, Jakarta)
Eddy (Department of Dental Materials, Faculty of Dentistry, Universitas Trisakti, Jakarta)
Thet Thet Swe (Department of Physics, University of Yangon, Yangon, Myanmar)



Article Info

Publish Date
01 Sep 2026

Abstract

Background: Bone grafting is a widely used technique in dentistry to repair bone defects. Limestone-based beta-tricalcium phosphate (β-TCP) holds potential as an alternative bone graft material when combined with polyacrylic acid (PAA) to produce composite blocks. Purpose: The aim of the study was to evaluate the characteristics, including porosity, diametral tensile strength (DTS), morphology, macropore size, and micropore size of block composites made from limestone-based β-TCP and PAA as well as the effect of their composition on these characteristics. Methods: This was a laboratory experimental study employing a post-test-only control group design. The study groups consisted of a negative control (pure PAA powder), a positive control (PAA + commercial β-TCP), and three treatment groups with variations in the mixture of limestone β-TCP and PAA: 60:40, 50:50, and 40:60 (%w/w). The samples were characterized for porosity using volume and weight measurements, for DTS using a universal testing machine, and for morphology using scanning electron microscopy. Results: Limestone-based β-TCP produced composites with higher porosity and DTS compared to pure PAA samples and commercial β-TCP. Increasing the β-TCP content generally increased porosity and DTS, although porosity decreased in the 40:60 group. The composite blocks predominantly exhibited closed porosity, with macropore size ranging from 81.30 µm to 198.40 µm. Conclusion: Increasing the proportion of limestone-based β-TCP results in higher porosity and DTS values than commercial β-TCP, partly due to particle size contributing to higher values. The composite blocks are porous, while pure PAA has a smooth, pore-free surface. However, further optimization is still required.

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Journal Info

Abbrev

MKG

Publisher

Subject

Dentistry

Description

The Dental Journal (Majalah Kedokteran Gigi) (e-ISSN:2442-9740; p-ISSN:1978-3728) is published by the Faculty of Dental Medicine, Universitas Airlangga. Its diciplinary focus is dental science and dental hygiene. The Dental Journal (Majalah Kedokteran Gigi) is published in English on a quarterly ...