Functional material of iron oxide (Fe2O3) nanoparticles-functionalized Hydroxyapatite (HA) was synthesized from chicken bone waste. The preparation of material involved the calcination of chicken bone waste followed by the dispersion of iron oxide precursors and hydrothermal treatment to get coprecipitated HA. Systematic physicochemical characterization was performed by various analytical techniques, including scanning electron microscopy, transmission electron microscopy, X-ray diffraction, Raman spectroscopy, and diffuse reflectance UV-Visible spectroscopy. The photocatalytic activity of the composite was examined to degrade methylene blue under various photon sources and pH condition. The results demonstrated that a high crystalline Fe2O3/HA was derived, and detail of the analysis confirm the functionality of iron as dopant in the crystalline structure of HA and the dispersed photoactive nanoparticles. Photocatalytic degradation experiments resumed that the high degradation efficiency could be achievable at alkaline condition and under visible light illumination, as the efficiency of 78.88% was the optimum value. Copyright © 2026 by Authors, Published by BCREC Publishing Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).
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