Warta IHP (Warta Industri Hasil Pertanian)
Vol 13, No 1-2 (1996)

(Method of Separation of Acetone-Butanol-Ethanol from Fermentation Broth By Fractional Distillation)

Moestafa, Achmad (Balai Besar Industri Agro)
Gumbira sa’id, E (Balai Besar Industri Agro)
Suparno, Sri Wuri Handono (Balai Besar Industri Agro)
Sukarno, Lalu (Balai Besar Industri Agro)



Article Info

Publish Date
07 Jul 2017

Abstract

Acetone-butanol-etanol (ABE) mixture in fermentation broth drived from fermentation of empty bunch of palm fruit is still containing butyric and acetic acid.The mixture can be separated by into its components byfractional distillation based on their different boilling points.The presence of butyric and acetic acid in the broth liquid did not interfere the yield of distillation. It was beneficial to concentrate the ABE content before the real fractional distillation was taken place.By collecting 12% of the liquid through a simple distillation had increased the concentration of ABE mixture from 17.42 to 125.25g/1.Fractionation of concentrated ABE mixture at 45 to 65 degree C on 3:1 reflux ratio produced aceton with concentration 554.63 g/1 and purity 70.22% while those of etanol at 78 to 81 C on  30:1 reflux ratio produced 424.73 g/1 and purity 53.61%.The residue was consist of water and and water was distilled like a stem distillation,since butanol has higher boiling point than water and the distillate was separated base on their different density.The yield of butanol 709.15 g/1 and purity 87.57%.

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Journal Info

Abbrev

ihp

Publisher

Subject

Agriculture, Biological Sciences & Forestry Industrial & Manufacturing Engineering

Description

Warta IHP (Industri Hasil Pertanian) is a Scientific Journal which is sourced from research papers, new theoretical/interpretive findings, and critical studies or reviews (by invitation) in the agro-based industry scope that cover any discipline such as: food science and technology, agricultural ...