Indonesian Mining Journal
Vol 8, No 01 (2005): INDONESIAN MINING JOURNAL Vol. 8 No. 1 February 2005

SYNTHESIS OF Na-A ZEOLITE FROM NATURAL ZEOLITES

Sariman Sariman (R & D Centre for Mineral and Coal Technology)



Article Info

Publish Date
14 Jun 2017

Abstract

Conversion of natural zeolites into Na-A zeolite by the two-step method has been achieved. Synthesis process was conducted at hydrothermal condition 90° and 100° C using alkaline silicates as silica source aluminate as alumina source. The silica was derived from zeolitic tuff and the sodium aluminate was obtained from chemical reagent. Dissolution on zeolitic tuff was made in order to obtain supernatant, Na2SiO3.nH2O. Reaction time for the synthesis ranged from 0.5 – 4 h. It is found that SiO2/Al2O3 molar ratio of 1.6, Na2O/SiO2 molar ratio of 4.41, and Na2O/H2O molar ratio of 60.70, and crystallization time of 4 h give maximum crystallinity. XRD and SEM showed that Na-A zeolite synthesis begins after 1 h and reaches its crystallization maximum. Then Na-A is substituted by Na-X and hydroxysodalite (HS) zeolite. The XRD pattern and SEM image show that microtextural are comparable to the reputed zeolite commercial.

Copyrights © 2005






Journal Info

Abbrev

imj

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Earth & Planetary Sciences Energy Engineering Environmental Science

Description

This Journal is published periodically two times annually : April and October, containing papers of research and development for mineral and coal, including exploration, exploitation, processing, utilization, environment, economics and policy. The editors only accept relevant papers with the ...