Jurnal Purifikasi
Vol 10 No 1 (2009): Jurnal Purifikasi

CHROMIUM AND LEAD REMOVAL USING SYNTHESIZED NANOCRYSTALLINE ZEOLITE

Izarul Machdar (Unknown)



Article Info

Publish Date
11 Apr 2018

Abstract

Zeolite Y nanocrystal was synthesized from a clear solution at temperature of 80-1500C with 6.38 of Si/Al molar ratio by using Aluminum isopropoxide (Al(OiPr)3) and Ludox LS as alumina and silica source, Tetrametylammonium Hidroxide (TMAOH) and Tetrametylammonium Bromide (TMABr) as first and second organic template, respectively. The products were characterised by X-Ray Diffractometer (XRD) and Scanning Electron Microscopy (SEM) to identify the structure and particle sizes. The image measurements of the particle size record that the average particle sizes of FAU-5, FAU-20 and FAU-35 are 116.46 nm, 169.33 nm and 178.12 nm, respectively. Furthermore, 0.5988 g and 0.6001 g of yields with average particle sizes of 116.46 nm and 43.76 nm can be obtained for FAU-5 (single organic template) and FAU-10 (two organic template, TMABr/TMAOH=0.15) samples, respectively. The smallest average particle size observed is 33.87 nm (FAU-15). The synthesised nanocrystalline zeolite Y was applied for Pb(II) and Cr(III) removal and the results show that the nano crystal samples have very good performance. On FAU-37 at 10 ppm, 30 ppm, 50 ppm and 80 ppm of initial concentration, the adsorption of Pb is 23.56 mg/g, 109.71 mg/g, 181.02 mg/g and 231.46 mg/g, respectively at 216 h and adsorption capacities of Cr are 23.18 mg/g, 84.94 mg/g, 109.75 mg/g and 147.37 mg/g.

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Journal Info

Abbrev

purifikasi

Publisher

Subject

Chemical Engineering, Chemistry & Bioengineering Environmental Science

Description

Jurnal Purifikasi was published since January 2000 by Division of Journal Purifikasi Department of Environmental Engineering-Faculty of Civil, Environment and Geo Engineering. Institut Teknologi Sepuluh Nopember, Surabaya in collaboration with the Association of Indonesian Sanitary and Environmental ...