Teknologi Indonesia
Vol 39, No 2 (2016)

FLOW RATE OF CARRIER GAS AFFECTING THE KEY PARAMETERS OF GC-TCD FOR CO2, C3H8, AND CO ANALYSIS: AN EXPERIMENTAL INVESTIGATION

Zuas, Oman (Unknown)
Budiman, Harry (Unknown)



Article Info

Publish Date
12 Oct 2016

Abstract

This paper reports on the effect of flow rate of helium (He) carrier gas on the key parameters of gas chromatography equipped with thermal conductivity detector (GC-TCD) for the measurement of carbon dioxide (CO2 ), propane (C3H8) and carbon monoxide (CO) in gravimetric standard gas mixture (Grav-SGM). The carrier gas has a function to transport vaporized molecules through the column during the GC separation process. The study provides opportunity to experimentally investigate the effect of gas flow rate on the several key parameters of the GC-TCD including retention time, peak area, peak height, response factor, resolution and selectivity. The results show that all key parameters were found to be carrier gas flow rate dependent. The increase of the gas flow rate could significantly decrease the retention time, peak area and response factor of the gas components. While both resolution and selectivity factor were observed to have a substantial decrease with increasing the flow rate of carrier gas. Therefore, proper selection of flow rate level of carrier gas is suggested before a GC measurement is carried out for obtaining an optimum condition.

Copyrights © 2016






Journal Info

Abbrev

JTI

Publisher

Subject

Computer Science & IT

Description

JTI is a journal in the Departement of Engineering Sciences - Indonesian Institute of Sciences (LIPI). JTI has policy to publish a new and original research paper or a review paper in The scope of Technology. JTI publishes two issues per year. The journal has been registered with printed-ISSN ...