INTEK: Jurnal Penelitian
Vol 5 No 1 (2018): April 2018

Pengaruh Metode Sintesis Silika Mesopori SBA-15 terhadap Analisis Differential Scanning Calorimetry dan Pengukuran Low Angles X-Ray Diffraction

Ridhawati, Ridhawati (Unknown)
Wahab, Abdul Wahid (Unknown)
La Nafie, Nursiah (Unknown)
Raya, Indah (Unknown)



Article Info

Publish Date
29 Apr 2018

Abstract

Mesoporous silica SBA-15 is an interesting material having highly ordered nanopores and large surface area, which is synthesized by sol gel and hydrothermal methods. In this study, mesoporous silica SBA-15 was synthesised with two different methods and the characteris was using X-Ray Diffraction (XRD) and Differential Scanning Calorimetry (DSC). SBA-15 was prepared TEOS as precursor and Pluronic 123 as surfactant. Thermoporous mesoporous DSC thermogram results of the SBA-15A mesoporous silica is (Tg 79oC and Tc 158oC). This is relatively lower than SBA-15B (Tg 86oC and Tc 158oC). The measurement of low angle X-Ray Diffraction SBA-15A has a crystal size 9.46 nm and SBA-15B has a crystal size 9.96 nm. The synthesis of SBA-15 using the hydrothermal method needs to be studied further to obtain thermal characteristics and a more stable crystal structure

Copyrights © 2018






Journal Info

Abbrev

Intek

Publisher

Subject

Computer Science & IT Engineering

Description

INTEK is a journal managed by the Journal and Publication Development Unit of Ujung Pandang State Polytechnic, which is published twice a year, in April and October. The journal INTEK has also been indexed. The INTEK Journal accepts research scripts in the fields of technology and engineering such ...