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CHEESA: Chemical Engineering Research Articles
Published by Universitas PGRI Madiun
ISSN : 26148757     EISSN : 26152347     DOI : -
Core Subject : Science, Engineering,
Chemical Engineering, Chemistry & Bioengineering Chemistry
CHEESA: Chemical Engineering Research Articles is scientific journal that publishes articles in the field of Chemical Engineering, Organic Chemistry, Inorganic Chemistry, Analytical Chemistry, Biochemistry, and Physical Chemistry. It is a journal to encourage research publication to research scholars, academicians, professionals and student engaged in their respective field. Author can submit manuscript by doing online submission. Author should prepare their manuscript to the instructions given in Author Guidelines before doing online submission. Template of article can be download in right sidebar. All submissions will be reviewed and evaluated based on originality, technical research, and relevance to journal contributions. Chemical Engineering Research Articles is published by Universitas PGRI Madiun on June and December.
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Articles 1 Documents
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Search results for , issue "Vol. 9 No. 1 (2026): In Progress" : 1 Documents clear
Green Synthesis of CuO-Doped Fe₃O₄ for Degradation of Crystal Violet Dye: RSM-Based Optimization Mara, Ady; Riyanti, Fahma; Desnelli; Hariani, Poedji Loekitowati
CHEESA: Chemical Engineering Research Articles Vol. 9 No. 1 (2026): In Progress
Publisher : Universitas PGRI Madiun

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25273/cheesa.v9i1.24394.1-14

Abstract

The limitations of CuO photocatalyst include high electron–hole recombination and low charge-transfer efficiency. In this context, doping with Fe3O4 is used to form a heterojunction, which enhances charge separation, increases electron transfer, and imparts magnetic properties for easy separation and reuse of the catalyst. Therefore, this study aimed to synthesize a biphasic CuO/Fe₃O₄ composite using Rhodomyrtus tomentosa leaf extract as a green reducing agent, and evaluate the performance as a photocatalyst for the degradation of Crystal Violet Dye (CVD). Structural, morphological, optical, and magnetic properties were characterized using X-ray diffraction (XRD), scanning electron microscopy with energy-dispersive X-ray spectroscopy (SEM–EDX), UV–Vis diffuse reflectance spectroscopy (DRS), and vibrating sample magnetometer (VSM). XRD patterns confirmed the coexistence of CuO and Fe₃O₄ phases, indicating successful composite formation. VSM analysis reported that the composite had magnetic properties with a saturation magnetization and band gap values of 46.92 emu/g and 1.63 eV, respectively. Process optimization was conducted using Response Surface Methodology (RSM) based on Central Composite Design (CCD). The results showed that the quadratic model was the most appropriate and statistically significant model, indicated by a p-value < 0.05 with a coefficient of determination (R2) of 0.9953. In addition, optimization of the degradation process led to CVD degradation efficiency of 98.73% under optimal conditions of initial concentration of 25.4 mg/L, pH 9.5, and irradiation time of 39.4 min with a visible-light radiation source. The composite also reported good reusability, retaining 92.11% of degradation efficiency after five cycles, confirming the potential as a magnetically recoverable, environmentally sustainable photocatalyst for wastewater treatment applications.

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