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Atom Indonesia Journal
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Exist for publishing the results of research and development in nuclear science and technology Starting for 2010 Atom Indonesia published three times a year in April, August, and December The scope of this journal covers experimental and analytical research in all areas of nuclear science and technology. including nuclear physics, reactor physics, radioactive waste treatment, fuel element development, radioisotopes and radio pharmaceutical engineering, nuclear and radiation safety, neutron scattering, material science and technology, as well as utilization of isotopes and radiation in agriculture, industry, health and environment.
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Articles 7 Documents
Search results for , issue "Vol 36, No 2 (2010): August 2010" : 7 Documents clear
Simpler and More Accurate: Weighing the Mercury in Electrolytic Cells by Radiotracer Dilution Method Sugiharto Sugiharto; S.B. Santoso; G.B. Santoso
Atom Indonesia Vol 36, No 2 (2010): August 2010
Publisher : PPIKSN-BATAN

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (194.049 KB) | DOI: 10.17146/aij.2010.22

Abstract

Weight of mercury in electrolytic cell of soda industry is usually measured gravimetrically, which is typical labor work in character. Error sources of the gravimetric method might have come from the fact that some mercury’s are usually trapped in the cell due to complicated structure of electrolytic cell. This cause unknown errors. In addition, formation of amalgam at the cathode may cause a further uncertainty in the measurement. Total error from gravimetric method is 4% on average. Radiotracer dilution method provides advantages either for simplification of procedure and reduction of measurement error. In this experiment radioisotope mercury 203Hg, which was prepared in nuclear reactor was used to examine 13 of 14 electrolytic cells of soda plant. Each electrolytic cell was designed containing approximately 700 kg inactive mercury. Before injection, the radioisotope mercury was mixed with non radioisotope mercury in a bath to obtain a suitable injection aliquots and standard references. Calibration curve, which was derived from two stage dilution processes taken from standard references, was used to examine degree of mixing between radioisotope and non radioisotope mercury and it was also used in weight calculation of non radioisotope mercury in electrolytic cell. Injection was carried out simply by pouring the injection aliquots into the flowing mercury at the inlet side of the cell. Mercury samples from the cells were extracted at regular time intervals and filled into vials for counting. This was done for the primary conformation of the completeness of mixing of the tracer with the non radioisotope mercury in each cell. When complete mixing is achieved, the unknown quantity of mercury in each cell was calculated based on mass balance principle. From the calculation the weight of mercury in each electrolytic cell was not the same and maximum error of measurement obtained from this method is 2.48 %. Compared to gravimetrically error mentioned above, it was clear that radiotracer dilution method gives better result in terms of higher accuracy and simpler procedure in measurement of the weight of mercury in electrolytic cells. Above all, this method is very suitable to be implemented in soda industry.Received: 20 November 2009; Revised: 31 August 2010; Accepted: 31 August 2010
The Role of X-Ray Diffraction for Analyzing Zr-Sn-Nb-Fe Alloys as Power Reactor Fuel Cladding Sugondo Sugondo
Atom Indonesia Vol 36, No 2 (2010): August 2010
Publisher : PPIKSN-BATAN

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (275.35 KB) | DOI: 10.17146/aij.2010.24

Abstract

Synthesis of Zr-1%Nb-1%Sn-1%Fe alloy is undertaken in order to develop fuel cladding alloy at high burn-up. Powder specimens of Zr-Sn-Nb-Fe alloy were prepared and then formed into pellets with a dimension of 10 mm in height 10 mm in diameter using a pressure of 1.2 ton/cm2. The 5 gram green pellets were then melted in an arc furnace crucible under argon atmosphere. The pressure in the furnace was set at 2 psi and the current was 50 A. Afterwards, the ingots were heated at a temperature of 1100°C for 2 hours and subsequently quenched in water. The ingots then underwent annealing at temperatures of 400°C, 500°C, 600°C, 700°C, and 750°C for 2 hours. The specimens were analyzed using X-ray diffraction in order to construct diffractograms. Results of the diffraction patterns were fitted with data from JCPDF (Joint Committee Powder Diffraction File) to determine the type of crystals in the elements or substances. The greater the crystallite dimension, the smaller the dislocation density. Agreeable results for hardening or strengthening were obtained at annealing temperatures of 500°C and 700, whereas for softening or residual stress at 600°C and 750°C. The nucleation of the secondary phase precipitate (SPP) was favourable at annealing temperatures of 400°C, 500°C, and 700°C. For Zr-1%Nb-1%Sn-1%Fe alloy with annealing temperatures between 400°C to 800°C, precipitates of Fe2Nb, ZrSn2,FeSn, SnZr, NbSn2, Zr0.68Nb0.25Fe0.08, Fe2Nb0.4Zr0.6, Fe37Nb9Zr54, and ω-Zr were observed. Satisfactory precipitate stabilization was achieved at annealing temperature of 800°C, growth of precipitates at temperature between 500°C to 600°C, and minimization of precipitate size at 700°C.Received: 20 November 2009; Revised: 31 August 2010; Accepted: 31 August 2010
The Effects of Gamma Irradiation on the Growth and Propagation of In-Vitro Chrysanthemum Shoot Explants (cv. Yellow Puma) I. Dwimahyani; S. Widiarsih
Atom Indonesia Vol 36, No 2 (2010): August 2010
Publisher : PPIKSN-BATAN

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/aij.2010.25

Abstract

The study on the effect of gamma irradiation on in-vitro shoot growth of chrysanthemum cv. Yellow Puma has been carried out. The aim of the study was to observe genetic variability of shoot growth caused by gamma irradiation. Shoot explants with four leaves were irradiated by gamma with dose of 10, 15 and 20 Gy with 3 replications at each of dose. The irradiated shoot explants were then transferred into fresh MS solid medium and placed in a growth room. Observation was performed on number of leaves and branches on M1V0 generation, while plantlets height and number of branches were observed a M1V1 generation. Number of survival plantlets and multiplication rate on three subsequent subcultures were observed as well. Results showed that gamma rays with dose of 20 Gy inhibited growth of leaves as much as 50% compared to control (shoots without irradiation), and branches 73.7% in three weeks. Observation on multiplication rate at M1V1 generation showed that gamma irradiation with dose of 10 Gy promoted multiplication rate as much as 10% higher than control. It can be concluded that in vitro mutagenesis using gamma iradiation with dose of 10 to 15 Gy can be used for inducing genetic variability of chrysanthemum cv. Yellow Puma. Received: 18 December 2008; Revised: 10 August 2010; Accepted: 30 August 2010
Measurement of P Contribution From Several P Sources by Using 32P Method A.D. Suyono; A. Citraresmini
Atom Indonesia Vol 36, No 2 (2010): August 2010
Publisher : PPIKSN-BATAN

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/aij.2010.19

Abstract

P-fertilizer other than chemical fertilizers has been used extensively in agriculture. However, the extent to which P-fertilizer contributes to the growth of plants has only been discussed a few, meanwhile the information will be very helpful to the use of P-fertilizer efficiently. The 32P method was used to distinguish P contribution from several sources, i.e soil, chemical fertilizer (Sp) and manure/organic fertilizer (Pk). The isotope carrier free solution of KH232PO4, which is contained of 98% 32P, was applied to the soil and thus making it as the only source of labeled-P. Radioactivity counting of soil samples will lead to the measurement of P-contribution from several sources of P given. The experiment result showed that most of the P taken up by the plants was from soil. Thus, the P from Sp (P-Sp) and Pk (P-Pk) became un-significantly support the plant growth expressed in lesser dry weight of straw, grain and plants compared to those who taken its P from soil. Although soil contributed most of its available P to straw and grain of lowland rice, but Sp and Pk still contributed P to both plant parts. It was obtained that in straw 64 – 82% P was derived from soil; 12 – 21% P was derived from Pk; and 18 – 29% P was derived from Sp. For grain 49 – 89% P was derived from soil; 11 – 15% P was derived from Pk; and19 – 45% P was derived from Sp. Received: 20 November 2009; Revised: 09 August 2010; Accepted: 23 August 2010
The Importance of Magnetic Reflection Condition and Polarization Factor: Case Study of MnF2 A. Purwanto
Atom Indonesia Vol 36, No 2 (2010): August 2010
Publisher : PPIKSN-BATAN

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/aij.2010.238

Abstract

Neutron diffraction has been widely accepted as a versatile tool to investigate magnetic structure of crystalline materials, which contribute significantly to the scientific and technological advances. Starting from a general formulation of the magnetic structure factor, one can often simplify the formulation depending on the crystallographic structure and the magnetic wave propagation vector of the sample. The simplification allows magnetic moment coupling and polarization deduction without the need of the refinement process. This paper elaborates such simplification for MnF2 to provide the determination of the magnetic moment coupling and polarization direction simply based on the reflection condition and polarization factor. The determination of the magnetic structure excluding its magnitude by the reflection condition and polarization factor is much more conclusive than by any magnetic structure refinement. Furthermore, MnF2 illustrates a rare compound that has antiferromagnetic structure with zero magnetic wave propagation vector, i.e.; it has the same antiferromagnetic and crystallographic unit cell.Received:19 May 2009; Received: 30 August 2010; Accepted: 31 August 2010
Monitoring Low-Cycle Fatigue Material-Degradation by Ultrasonic Methods R. Himawan; H. Katoh; A. Cahyono
Atom Indonesia Vol 36, No 2 (2010): August 2010
Publisher : PPIKSN-BATAN

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/aij.2010.26

Abstract

Any system consisting of structural material often undergoes fatigue, which is caused by dynamic load cycle. As a structural system, nuclear power plant is very likely to have low-cycle fatigue at many of its components. Taking into account the importance of monitoring low-cycle fatigue on structural components to prevent them from getting failure, the authors have conducted a work to monitor material degradation caused by low-cycle fatigue by using ultrasonic method. An alloy of Cu-40Zn was used as a test specimen. Ultrasonic water immersion procedure was employed in this ultrasonic test. The probe used is a focusing type and has frequency as high as 15 MHz. The specimen area tested is in the middle part divided into 14 points × 23 points. The results, which were frequency spectrums, were analyzed using two parameters: frequency spectrum peak intensity and attenuation function gradient. The analysis indicates that peak intensity increases at the beginning of load cycle and then decreases. Meanwhile, gradient of attenuation function is lower at the beginning of fatigue process, and then consistently gets higher. It concludes that low-fatigue material degradation can be monitored by using ultrasonic method.Received: 20 November 2009; Revised: 31 August 2010; Accepted: 31 August 2010
Molecular Identification of Mycobacterium tuberculosis and Analysis of Its Resistance to Rifampin in Sputa From Tuberculosis Suspected Patients M. Syaifudin
Atom Indonesia Vol 36, No 2 (2010): August 2010
Publisher : PPIKSN-BATAN

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/aij.2010.20

Abstract

An accurate identification of different species of Mycobacterium provides to allow appropriate treatment for Mycobacterium tuberculosis infection. Beside that, drug resistance of M. tuberculosis strains to rifampin is not clearly understood in contributing to the spread of tuberculosis in Indonesia. To assess the molecular mechanism of rifampin resistance, a number of clinical specimens of M. tuberculosis were analyzed their molecular nature of a part of the rpoB gene using polymerase chain reaction-single strand conformation polymorphism (PCR-SSCP) methods. DNA’s extracted from sputum samples were amplified and 32P-labeled by PCR with the specific primers and the product was analyzed their mutation conferring resistance by MDE gel electrophoresis. Of the 70 specimens tested, 57 specimens were positive for M. tuberculosis organism only, three specimens contained a mixture of M. tuberculosis and non tuberculosis mycobacteria (NTM), and 10 specimens were negative approved by Duplex PCR. Of these sixty DNA positive samples (thus the sensitivity of PCR was 85.71%), 5 (8.3%) of them suspected to contain mutations in rpoB which were associated with rifampin resistance. Even though the frequency of mutation was low, the results from our study clearly indicate that the molecular mechanism of rifampin resistance in M. tuberculosis isolates from Indonesia involves alterations in the rpoB gene. Molecular diagnosis by PCR which is fast and easy to perform is useful for early and rapid detection of TB in sputum specimen. Received: 27 February 2009; Revised: 28 August 2010; Accepted: 30 August 2010

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