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Jurnal Sains Materi Indonesia

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Published by Badan Tenaga Nuklir Nasional

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Core Subject : Science,

Materials Science & Nanotechnology

Jurnal Sains Materi Indonesia (Indonesian Journal of Materials Science), diterbitkan oleh Pusat Teknologi Bahan Industri Nuklir - BATAN. Terbit pertama kali: Oktober 1999, frekuensi terbit: empat bulanan.

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Articles 10 Documents

Search results for , issue "Vol 21, No 1: OCTOBER 2019" : 10 Documents clear

Microstructure of Oxide Dispersion Strengthened Steel With Cr Content Variation Marzuki Silalahi; Bernadus Bandriyana; Arbi Dimyati; Bambang Sugeng; Syahfandi Ahda; Fitria N
Jurnal Sains Materi Indonesia Vol 21, No 1: OCTOBER 2019
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Microstructure and phase distribution of innovative Oxide Dispersion Strengthened (ODS) steel based on Fe-Cr-ZrO2 particularly for application at high temperature reactor with variation of Cr content was analysed. The alloy was synthesized with Cr composition variation of 15, 20 and 25 wt.% Cr, while zirconia dispersoid kept constant at 0.50 wt.%. The samples was synthesized by mechanical alloying comprising of high energy milling for 3 hours followed by vibrated compression with iso-static load at 20 ton. The final consolidation was performed via sintering process for 4 minutes using the Arc Plasma Sintering (APS) technique, a new method developed in BATAN especially for synthesizing high temperature materials. The samples were then characterized by means of scanning electron microscopy (SEM) with energy dispersed X-ray (EDX) analysis capability and X-ray diffraction. The mechanical property of hardness was measured using standard Vickers micro hardness tester to confirmed the microstructure analysis. The results show that the microstructure of the ODS alloy samples in all variation of Cr content consists generally of cubic Fe-Cr matrix phase with small of porosity and Zirconia particles distributed homogenously in and around the matrix grains. The achievable hardness was between 142 and 184 HVN dependent consistently on Cr content in which Cr element may cause grain refining that in turn increase the hardness.

Calculated Radioactivity Yields of Gallium-67 using Matlab Codes Imam Kambali
Jurnal Sains Materi Indonesia Vol 21, No 1: OCTOBER 2019
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

In nuclear medicine, gallium-67 (67Ga) is potentially applied for imaging a certain type of tissue. In this investigation, 67Ga is theoretically studied in terms of its potential radioactivity yields at the end of various energetic proton bombardments. Nuclear cross-sections derived from the Talys Evaluated Nuclear Data Library (TENDL) 2017 were used as the input files, while a Matlab code was developed to perform the yield calculations of 67Zn(p,n)67Ga and 68Zn(p,2n)67Ga nuclear reactions to produce 67Ga. Two different targets – enriched 67Zn and natZn targets – were simulated in the calculations. The calculated yields suggested that a maximum of 27.37 MBq/µAh could be achieved when enriched 67Zn target was irradiated with 15-MeV protons, whereas 46.99 MBq/µAh could be generated following a 30 MeV proton bombardment of enriched 68Zn target. Various radioactive gallium impurities, i.e. 63,64,65,66,68,70Ga and stable 69Ga isotope were also expected to be generated mostly via (p,n) and (p,2n) reactions when natZn target was used in the 67Ga production. In contrast, radioactive 66Ga and 68Ga impurities were mainly produced following bombardment of enriched 67Zn and 68Zn targets. This study can be used as a reference for future 67Ga radionuclide production.

ELECTROCHEMISTRY STUDY ON THE RELATIONSHIP BETWEEN GRAIN BOUNDARY STATE AND CORROSION BEHAVIOR OF ULTRAFINE GRAINED IRON CHROMIUM ALLOY Ahadi Damar Prasetya; Muhammad Rifai; Ahmad Hasan As'ari; Mujamilah Mujamilah; Hiroyuki Miyamoto
Jurnal Sains Materi Indonesia Vol 21, No 1: OCTOBER 2019
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

ELECTROCHEMISTRY STUDY ON THE RELATIONSHIP BETWEEN GRAIN BOUNDARY STATE AND CORROSION BEHAVIOR OF ULTRAFINE GRAINED IRON CHROMIUM ALLOY. Research on stainless steel corrosion resistance continues to grow today. This reality cannot be separated from the needs of stainless steels in various fields, one of which is bio-implant. In this research, the effect of grain size on the corrosion behavior of iron-chromium (Fe-Cr) alloy was investigated. Coarse grain Fe-Cr alloy was first processed with equal channel angular pressing (ECAP) for eight cycles to obtain ultrafine grain structure. The coarse and ultrafine grain samples then were then tested using XRD, SEM-EBSD, and the pitting corrosion properties tested using potentiodynamic polarization method in NaCl 1 M solution. The result of XRD dan SEM-EBSD shows that the initial sample is truly has a coarse grain structure, while ECAP produces an ultrafine grain structure. Corrosion test results showed that the ultrafine grain sample had better pitting corrosion resistance compared to the coarse grain sample. This behavior is related to the rate of passivation that depends on non-equilibrium grain boundaries, which can be easily observed in the ultrafine grain structure. Based on these results, it can be concluded that the ultrafine grain Fe-Cr alloy has a better corrosion resistance compared to the coarse grain.

Isotherm, Thermodynamic, and Kinetics Studies of Iodide Adsorption on The Al_SBA-16 Mesoporous Nanomaterial as Radiopharmaceutical Vehicle Candidate Maria Christina Prihatiningsih; Sri Sundari Retnoasih; Athanasia Elra Andjioe; Noor Anis Kundari; Edy Giri Rachman Putra
Jurnal Sains Materi Indonesia Vol 21, No 1: OCTOBER 2019
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

In order to investigate the potential of Al_SBA-16 Mesoporous Nanomaterial as a candidate for radiopharmaceutical vehicles, the studies of kinetics, thermodynamic, and in vitro stability of Iodide adsorption onto the nanomaterial have been carried out. The adsorption study was conducted at different temperature, time, and iodide concentration and observed with spectrophotometric techniques. The isotherm adsorption was fitted with Langmuir and Freundlich model and the thermodynamic parameters were determined at temperatures of 293K, 301K, 308K, and 313K. Moreover, the adsorption kinetics was analyzed in terms of pseudo first order model for Al_SBA-16 Mesoporous Nanomaterial and Iodide and pseudo second order in overall reaction. The activation energy was determined by using Arrhenius equation, meanwhile, the in vitro stability testing was conducted in phosphate buffer saline at pH variation for 5.5 to 7.0, and at temperature variation for 20C to 45C and at testing time variation for 6 to 48 hours. The result indicate that the adsorption obeys the Langmuir isotherm model and has a tendency to be chemical adsorption with a value of H was -116.641 kJ/mol and the nature of spontaneous reactions. The adsorption process followed the pseudo-first-order model and the apparent activation energy was 41.26 kJ/mol. In the present research work, the in vitro stability data were evaluated using P-Value and the theory of Hypothesis Testing or Fisher's significance test. The result of hypothesis testing show that, the adsorption of iodide onto Al_SBA-16 Mesoporous Nanomaterial were highly stable under the experimental conditions adopted.

THE EFFECT OF RATIO OF GAS MIXTURE FOR MECHANICAL PROPERTIES AND CRYSTAL STRUCTURES ON 316L STAINLESS STEEL BIOMATERIAL USING DC SPUTTERING TECHNIQUE Wiwien Andriyanti; Bunyamin Arsyad; Ravendianto Ravendianto; Tjipto Sujitno; Suprapto Suprapto; Dwi Priantoro
Jurnal Sains Materi Indonesia Vol 21, No 1: OCTOBER 2019
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

316L stainless steel is widely used as an orthopedic implant due to its high corrosion resistance and biocompatibility, but the weakness of these materials is low hardness and high wear. The surface must be modified to improve the material. For the purpose, a titanium nitride (TiN) thin film was deposited on the surface of SS 316L using DC sputtering technique. The sputtering process was carried out for various of a gas mixture of argon (Ar) and nitrogen (N2) such as 90 Ar: 10N2, 80 Ar: 20 N2, 70 Ar: N2, and 60 Ar: 40 N2, while the other parameters kept constant. The objective of the gas mixture variation is to find out the optimum condition of ratio Ar: N2 gas mixture with the highest hardness and lowest wear resistance. From experiment done it’s found that the highest hardness in order of 232.02 VHN, while before being coated the hardness is 133.61 VHN, or there is an increasing hardness by factor 1.73, while the wear resistance reduces from 11.6 × 10-8 mm2/kg to 1.17 × 10-8 mm2/kg or there is reducing in wear resistance by factor 9.9. The optimum conditions were achieved at Ar: N2 ratio = 70:30. From XRD analysis, it can be concluded that the crystal structure of TiN thin film is cubic with the peaks (111), (200), (202), (311) and (222). From cross-section microstructure analysis using Scanning Microscope Electron (SEM), it’s found the thickness of the thin film is 744 nm.

Study of Microstructural and Corrosion Properties of Aluminium Alloy 7075 after Plasma Nitriding Haerul Ahmadi; Rizky Abdul Aziz; Suprapto Suprapto; Tjipto Sujitno; Sophie Hapsari
Jurnal Sains Materi Indonesia Vol 21, No 1: OCTOBER 2019
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Plasma nitriding is a treatment process of metals by depositing nitrogen into metal that considered to be nitrided by mean of increasing the mechanical, physical, and chemical properties of the metal. This treatment will form a hard layer compund of Al-N on the surface of the sample. In this study, aluminium alloy 7075 was nitrided which the application of it to structural part of aircraft makes it vulnarable to not only corrosion and wear attack but also decreasing the hardness of the material. One method to overcome these issues is plasma nitriding. The purpose of of this research is to do the characterizations of plasma nitrided aluminium alloy 7075 regarding its microstructure, mechanical, and chemical properties. The characterizations that had been done were microhardness Vickers testing, SEM-EDX, and electrochemical corrosion testing Potensiostat. The hardness of the sample increased 55% from 75,88 VHN (raw material) to 117,68 VHN (at optimum parameter). The depth of the white layer of plasma nitriding is approximately 6 µm, while the EDX result reported carbon, oxygen, and nitrogen presence. Corrosion testing showed that the highest corrosion rate is on the raw material, 0,15393 mpy. While the optimum one is 0,07184 mpy.

Growth of ZnS:Ag:Cu Thin Film Deposited on Glass Substrates using Thermal Evaporation Technique for Alpha-photovoltaic Emy Mulyani; Tjipto Sujitno; Dessy Purbandari; Ferdiansjah Ferdiansjah; Sayono Sayono
Jurnal Sains Materi Indonesia Vol 21, No 1: OCTOBER 2019
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

This paper presents the research on the growth of ZnS:Ag:Cu thin film on a glass substrate as a radio-luminescent material. The SRIM/TRIM software is used to determine the optimum thickness based on an energy deposition depth of 5.485 MeV Am 241 alpha radiation source on ZnS:Ag:Cu material. To increase the adhesive strength of the coating, initially, the glass substrate is etched using a plasma glow discharged at 280°C for 15 minutes. Multiple coatings of ZnS:Ag:Cu were etched on the glass substrate; this was carried out using a thermal evaporation technique to achieve the optimal thickness (based on SRIM/TRIM simulation). The thin film thickness was observed using a scanning electron microscope (SEM). The optical properties of the un-etched, etched glass substrate and thin-film were characterized using UV-Vis spectrometer. Based on SRIM/TRIM simulation, the optimal thickness is 22 mm which can be achieved by coating three times. From optical properties of ZnS:Ag:Cu thin film and after being analysed using Taue plot method, it is found that the energy gap of ZnS:Ag:Cu thin film is 2.48 eV. It can be concluded that the addition of Ag and Cu doped decrease the energy gap of ZnS (3.66 eV).

COVER JUSAMI VOL.21, NO.1, OCTOBER 2019 JUSAMI JUSAMI
Jurnal Sains Materi Indonesia Vol 21, No 1: OCTOBER 2019
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2019.21.1.6152

PREFACE JUSAMI Vol. 21, No. 1, October 2019 JUSAMI JUSAMI
Jurnal Sains Materi Indonesia Vol 21, No 1: OCTOBER 2019
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2019.21.1.6154

KEYWORD INDEX Jusami Jusami
Jurnal Sains Materi Indonesia Vol 21, No 1: OCTOBER 2019
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2019.21.1.6457

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