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Masruri
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Departemen Kimia, Fakultas MIPA, Universitas Brawijaya, Jl. Veteran 65145 Malang
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The Journal of Pure and Applied Chemistry Research
Published by Universitas Brawijaya
ISSN : 23024690     EISSN : 25410733     DOI : http://dx.doi.org/10.21776/ub.jpacr
Core Subject : Health, Science, Engineering,
Chemical Engineering, Chemistry & Bioengineering Chemistry Materials Science & Nanotechnology Medicine & Pharmacology
The Journal of Pure and Applied Chemistry Research focuses in publishing research articles in the field of Chemistry and Applied Chemistry. The target is in exploring, investigating, and developing chemicals sources from local and/or Indonesian to increase the value. Scope of the journal is organic chemistry, analytical chemistry, inorganic chemistry, biochemistry, and physical chemistry. Included the topic also organic chemistry natural product, theoretical and computational chemistry.
Arjuna Subject : Kimia(semua kategori) - Kimia (Lain-Lain)
Articles 7 Documents
 1 
Search results for , issue "Vol 11, No 3 (2022): Edition September-December 2022" : 7 Documents clear
Mini Electrode Based on Chitosan-Activated Carbon Membrane for Detection of Paracetamol in Herbal Medicine Ani Mulyasuryani; Rachmat Triandi Tjahjanto; Zainul Abidin
The Journal of Pure and Applied Chemistry Research Vol 11, No 3 (2022): Edition September-December 2022
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/ub.jpacr.2022.011.03.677

Abstract

A tube type mini electrode has been made to detect paracetamol levels in herbal medicine, the electrode is made of a glass tube with a diameter of 0.7 cm, a length of 3 cm. As the membrane is a mixture of chitosan, activated carbon from rice husk, and cetyl trimethyl ammonium (CTA)-paracetamol. The internal solution is a standard solution of 0.01 M paracetamol in a solution of phosphoric acid pH 2. The average sensitivity of the paracetamol sensor is (22.60 ± 0.01) mV/decade in a linear concentration range of 10-6 – 5x10-3 M, with an average recovery of (90.6 ± 0.5) %. Paracetamol sensor electrodes can be applied to samples of herbal medicine on the market, with an average error of (9.4 ± 0.1) %.
Study of Cu Recovery Comparison of Fresh, Stockpiled, and Mixed Ores Processing in Batu Hijau Mine – Sumbawa Island, Indonesia Surya Hadi; Agung Damar Syakti; Didik Supriadi Agustawijaya; Wahyu Dian Silviani; Karel Pramono; Rissa Anungstri; Jorina Waworuntu
The Journal of Pure and Applied Chemistry Research Vol 11, No 3 (2022): Edition September-December 2022
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/ub.jpacr.2022.011.03.691

Abstract

Batu Hijau mine is one of the mining areas in Indonesia that have been operated for 20 years. The main concentrate product in Batu Hijau contains the primary minerals copper (Cu) and gold (Au). However, the mine is not only processing the fresh mined ore but also store the low-grade ore in the stockpile. Therefore, this study compares the Cu recovery in different ore stockpile processing on and changes in the concentration of dissolved Cu in the tailings that potentially contaminated the environment. Chemical analysis of solid and dissolved Cu uses standard methods by strictly carrying out quality assurance and quality control (QA/QC) procedures to ensure the resulting data has high validity. The results showed that there is a slight increase in Cu’s solubility in liquid fraction of tailings and the recovery decrease when ores were processed from stockpiles. However, the recovery reduction is anticipated by flotation with controlled potential sulphidisation (CPS) using sodium hydrosulphide (NaHS). Besides, the CPS also ensure that only small amount of dissolved Cu that dumped in the tailings. Hence, the dissolved Cu concentration can be monitories to reduce the possible impact on the environment.
Synthesis of Struvite Crystal (MgNH4PO4.6H2O) from Laundry Waste to Consider its Potential as a Plant Fertilizer: Stirring and Processing Temperature Effect Dyah Suci Perwitasari; Nur Aini Fauziyah; Pardi Sampe Tola
The Journal of Pure and Applied Chemistry Research Vol 11, No 3 (2022): Edition September-December 2022
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/ub.jpacr.2022.011.03.697

Abstract

This paper aimed to process phosphate from laundry waste to be struvite crystal by precipitation and crystallization methods. In general, phosphates are difficult to remove by conventional treatment technologies. Therefore, precipitation and crystallization methods can be an alternative choice for phosphate recovery. Precipitation and crystallization methods can serve to remove dissolved phosphate content in wastewater, as well as convert it into a solid form that can be reused as industrial raw materials. The research variables used were stirring temperature (25, 30, and 35 °C) and stirring speed (100, 125, 150, and 200 rpm). By using X-ray Fluorescence (XRF) and Scanning Electron Microscope (SEM-EDX), the analysis showed that the highest percentage of phosphate removal was at a stirring speed of 100 rpm at 30°C, which was 47.5%. X-ray Diffraction (XRD) was also carried out on several samples and it was confirmed that the dominant crystal phase formed was a struvite (MgNH4PO4.6H2O) for all samples, and secondary phase Magnesium Phosphate Hydrate (Mg3(PO4)2*8H2O was found in a stirring speed of 100 rpm at 30°C. The morphology of the struvite crystals formed resembles irregular flakes by using SEM.
Iron Metal Ion Adsorption Capacity on Palm Oil Mill Effluent (POME) Using Montmorillonite Adsorbent Maria Dayanti Mellanie; Tisna Harmawan; Puji Wahyuningsih
The Journal of Pure and Applied Chemistry Research Vol 11, No 3 (2022): Edition September-December 2022
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/ub.jpacr.2022.011.03.657

Abstract

Palm oil mill effluent (POME) is the most produced waste among other types of waste, which is around 60% in every 100% processing of fresh fruit bunches containing heavy metals, namely ferrous metal (Fe). Montmorillonite (MMT) is one of the best adsorbents used to reduce the concentration of Fe in POME. In this study, the determination of the mass variation of the MMT as adsorbent and the variation of the contact time on the adsorption ability of Fe metal in POME was determined using an Atomic Absorption Spectrophotometer (AAS) and surface morphology analysis of MMT before and after adsorption using Scanning Electron Microscope (SEM). Based on the results of AAS analysis showed that greater the mass of the adsorbent then greater the amount of Fe from the POME that is adsorbed, and with variations in contact time that the longer the contact time between MMT and Fe then greater the amount of Fe in the palm oil mill effluent adsorbed on the adsorbent surface. The best adsorption conditions occurred at an adsorbent mass of 8.5 g MMT and a contact time of 5 hours with an adsorption capacity of 0.0383 mg/g. The results of the SEM showed the presence of empty spaces in the MMT before adsorption while after adsorption there were white granules that occupied the empty spaces evenly on the surface of the MMT. The granules indicate the presence of metals in the POME samples which are adsorbed on the MMT surface.
Synthesis and Characterization of Molecularly Imprinted Polymers (MIPs) Using Humic Acid Tikarahayu Putri; Muhammad Ali Zulfikar; Deana Wahyuningrum; Iwan Syahjoko Saputra
The Journal of Pure and Applied Chemistry Research Vol 11, No 3 (2022): Edition September-December 2022
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/ub.jpacr.2022.011.03.656

Abstract

MIPs was synthesized through microwave assisted organic synthesis (MAOS) method by using methyl methacrylate (MMA) as functional monomer, ethylene glycol dimethacrylate (EGDMA) as cross-linker, benzoyl peroxide (BPO) as initiator, N,N-dimethyl formamide (DMF) as porogen solvent, and (HA) as template. The MIPs was successfully synthesized according to the characterization using Fourier transform infrared (FTIR) spectroscopy, scanning electron microscope (SEM), electron dispersive spectrometer (EDS), and UV spectrophotometer. FTIR shows the other functional groups peaks in the FTIR spectra of NIPs and MIPs after leaching were appeared at the wavelength of 2955 cm-1 corresponded to stretching vibration of C-H of 1459 cm-1 and 1160.06 cm-1 corresponded to the vibration bands of CH3 and O-CH3. EDS shows the MIPs after leaching have the elemental compositions of C, O, and Si with a mass of 78.34, 21.43, and 0.23%. UV spectrum shows the MIPs and NIPs have absorbance values of 0.36 nm and 0.44 nm
Synthesis of Microsheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 via Molten NaCl-KCl Salt Method Anton Prasetyo; Andy Nur Muhammad Guntur; Suci Noerfaiqotul Himmah; Nur Aini; Usman Ali Rouf; Abdul Aziz
The Journal of Pure and Applied Chemistry Research Vol 11, No 3 (2022): Edition September-December 2022
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/ub.jpacr.2022.011.03.703

Abstract

Bi4Ti3O12 is a tri-layer Aurivillius member compound that was reported to have good photocatalytic properties. Metal element doping and morphological particle tuning are strategies to increase photocatalyst activity. In this research, the compound micro sheets Bi4Ti3O12 and Bi4Ti2.95V0.05O12 were synthesized using molten NaCl/KCl salt. The diffractogram shows that the Bi4Ti3O12 sample was successfully synthesized, however, there are still found impurities at the Bi4Ti2.95V0.05O12 sample. Micrographs showed that the morphology particle samples is. The results of UV-Vis DRS spectra calculation show that both samples have a band gap energy of ~2.97 eV.
Synthesis and Characterization of Cellulose Acetate and Nanocellulose Acetate from Sengon Agroindustrial Waste (Paraserianthes falcataria) Nur Ikhtiarini; Masruri MASRURI; Siti Mariyah Ulfa; Widodo Widodo
The Journal of Pure and Applied Chemistry Research Vol 11, No 3 (2022): Edition September-December 2022
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/ub.jpacr.2022.011.03.644

Abstract

Synthesis and characterization of cellulose acetate and nanocellulose acetate have been carried out. Cellulose was isolated from sengon wood powder waste using 6% NaOH solution and bleached with NaOCl. The cellulose was hydrolyzed with 60% formic acid to obtain nanocellulose. Cellulose and nanocellulose were then modified with acetic anhydride. The synthesized products were characterized by FTIR to identify organic functional groups, powder XRD to measure crystallinity, and SEM to observe surface morphology. Solubility tests in several types of solvents were also performed. The degree of substitution (DS) of cellulose acetate and nanocellulose acetate was carried out based on Indonesia’s SNI 0444:2009 method. The DS calculation show that the cellulose acetate and nanocellulose have DS of 2.9 and 2.1, respectively.

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