Rapid, non-destructive techniques for evaluating the internal quality of fresh oil palm fruit bunches (FFB) are needed to improve harvesting and postharvest management. This study aimed to develop predictive models for the moisture and oil content of fresh oil palm fruit bunches using electrical capacitance and chemometric analysis. Electrical capacitance (Cp) measurements were obtained using an inductance-capacitance-resistance (LCR) meter from fruit samples representing five maturity levels. The capacitance data were analyzed using Partial Least Squares Regression (PLSR) with several data preprocessing techniques, including Original, Baseline Correction, Standard Normal Variate (SNV), and Multiplicative Scatter Correction (MSC). Model performance was evaluated using the coefficient of determination (R²), the correlation coefficient (r), the standard error of prediction (SEP), the residual predictive deviation (RPD), and the consistency (%) parameter. Among the evaluated preprocessing methods, MSC produced the best model performance. The optimal model for moisture content was obtained using MSC with three latent factors, yielding R² = 0.74 r = 0.86, SEP = 5.02%, RPD = 1.81, and consistency = 86.12%. The optimal model for oil content prediction was also obtained using MSC with four latent variables, achieving R² = 0.88, r = 0.94, SEP = 3.84%, RPD = 2.36 and consistency = 93.84%. These results indicate that electrical capacitance combined with PLSR has potential as a rapid and non-destructive method for the chemical quality evaluation of oil palm FFB, particularly for oil content prediction, while moisture content prediction showed limited predictive capability.