Nur Fitri Fatimah
Program Studi Pendidikan Kimia FKIP Universitas Sebelas Maret

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Sintesis dan Analisis Spektra IR, Difraktogram XRD, SEM pada Material Katalis Berbahan Ni/zeolit Alam Teraktivasi dengan Metode Impregnasi Nur Fitri Fatimah; Budi Utami
JC-T (Journal Cis-Trans) : Jurnal Kimia dan Terapannya Vol. 1 No. 1 (2017)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um026v1i12017p035

Abstract

This research is about the synthesis and analysis of IR spectra, XRD difractogram, SEM in the catalyst material made from Ni/zeolite nature is activated by impregnation method. This study is aimed to find out (1) The method of synthesis of catalyst Ni/zeolit with impregnation (2) The characteristics of the catalyst which is formed from the characterization results using SEM, FT-IR, and XRD (3) the optimum ratio of zeolit and Ni in the synthesis of catalyst Ni/zeolit. Synthesis of catalyst Ni/zeolit were done by impregnation. Method with a variety of Ni concentration range 0 %, 5%, and 10%. Characterization of catalyst Ni/zeolit were produced covering the structure morphology and particle size using microgrpahy SEM (Scanning Electron Microscope). While characterization crystallization and the crystal size was performed using diffractogram of XRD (X-Ray Diffraction) and characterization with FT-IR. From this study it can be concluded that : (1) Ni/zeolit catalyst be synthesized from a solution of Ni(NO3)2.6H2O at variance 0%, 5%, and 10% with impregnation method, (2) characteristics of Ni/zeolit catalyst were identified using SEM analysis in the form of uneven surface morphology, the XRD, the peaks of Ni/zeolit cryztallinity and FT-IR