Muhammad Reza
Jurusan Kimia, FMIPA, Universitas Jember, Jember, Indonesia

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Penerapan Response Surface Methodology dalam Optimasi Kondisi Proses Ekstraksi Antosianin pada Limbah Kulit Kakao dengan Metode Maserasi Menggunakan Pelarut Etanol Istiqomah Rahmawati; Boy Arief Fachri; Nurtsulutsiyah Nurtsulutsiyah; Yakub Hendrikson Manurung; Muhammad Reza; Bekti Palupi; Meta Fitri Rizkiana; Helda Wika Amini
JC-T (Journal Cis-Trans) : Jurnal Kimia dan Terapannya Vol. 6 No. 1 (2022)
Publisher : Universitas Negeri Malang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17977/um0260v6i12022p024

Abstract

Anthocyanins are present in high concentration in cocoa peels. The purpose of this study is to identifythe relationship between each input variables and to develop predictive models used in optimizing theconditions of the anthocyanin extraction process. Extraction of anthocyanins in cocoa peels was carriedout using the maceration method. Extraction process conditions such as particle size (0,105; 0,125; 0,149;0,177; 0,25 mm), material/solvent ratio (0,0045; 0,0125; 0,0375; 0,0625; 0,0795 g/mL), and optimumextraction time (7,5; 24; 48; 72; 79 hour) in the extraction process will affect the obtained concentration ofanthocyanin. The Design Expert vs11 program with Response Surface Methodology (RSM) Box-BehnkenDesign was used for research and select process conditions from a combination of factors producing theoptimal responses. Relationship between variables and the response of anthocyanin concentration wasmodeled by Y=0,2129-0,0483A+0,0816B+0,0069C-0,0219AB-0,0271AC+0,0174BC+0,0298A2 -0,0349B2 +0,0504C2 (A is particle size; B is the ratio of cocoa peel/ethanol; and C is extraction time). The optimal response value of anthocyanin concentration is 0,479 M, with the condition of the particle size at the extraction process of 0,105 mm; the ratio of cocoa peel/ethanol of 0.0625 w/v; extraction time of 72 hours.