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All Journal Jurnal Inovasi Teknik Kimia Bulletin of Chemical Reaction Engineering & Catalysis
Khoiruddin, Wahib
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Chemical Engineering, Chemistry & Bioengineering Chemistry

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KATALIS KARBON YANG DIBUAT DENGAN METODE HUMMERS TERMODIFIKASI UNTUK ASETILASI GLISEROL Hidayati, Nur; Khoiruddin, Wahib; Mastuti, Isnadiah Endang; Pambudi, Wahyu Devi Satna
Jurnal Inovasi Teknik Kimia Vol 6, No 2 (2021)
Publisher : Fakultas Teknik Universitas Wahid Hasyim

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31942/inteka.v6i2.5445

Abstract

Gliserol adalah produk samping yang dihasilkan dari proses pembuatan biodiesel. Karena peningkatan produksi biodiesel, utilisasi gliserol yang melimpah menjadi asetin berpeluang dilakukan karena manfaat asetin sebagai sumber bahan baku untuk material lainnya yang bernilai lebih. Penelitian ini bertujuan untuk membuat katalis grafena oksida dari multi-walled carbon nanotubes (MWCNT) dengan menggunakan metode hummers termodifikasi. Karakterisasi katalis GO dilakukan dengan menggunakan uji X-Rays Diffraction (XRD) dan Scanning Electron Microscope-Energi Dispersive X-ray (SEM-EDX). Aktivitas katalitik pada asetilasi gliserol menunjukkan konversi yang tinggi mencapai 94% pada suhu 110°C dalam 2 jam reaksi dengan menggunakan katalis 3% berat
Synthesis and Characterisation of Graphene Oxide Catalysts for Glycerol Acetylation Hidayati, Nur; Khoiruddin, Wahib; Purnama, Herry; Effendy, Marwan
Bulletin of Chemical Reaction Engineering & Catalysis 2024: BCREC Volume 19 Issue 2 Year 2024 (August 2024)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.20146

Abstract

Glycerol in large quantities as a by-product of biodiesel production is a promising feedstock to be converted into more valuable products such as acetin. In this work, acetin converted from glycerol acetylation with acetic acid was performed over graphene oxide as a catalyst in a batch reactor. The study's objective was to evaluate the effect of sodium nitrate amount in the catalyst preparation on the catalyst's characteristics and catalytic performance. The graphene oxide (GO) catalysts were charac­terised by various tests, such as SEM-EDX for their morphology, the nitrogen adsorption capacity using Breneur-Emmet Teller (BET), structural analysis using XRD, functional group us­­ing FTIR, and catalytic activity on glycerol acetylation. The GO1, GO2, and GO3 catalysts were varied based on the NaNO3 amount in the modified Hummer method. The experiments found that the NaNO3 amount in catalyst preparation plays a vital role in GO structure formation. The GO2 catalyst has the highest performance, as indicated by the highest surface area, pore volume, and size. High glycerol conversion (94 %) and selectivity toward the interest products of triacetin (24 %) and diacetin + triacetin (83 %) were reached in 2 h of reaction using three wt.% catalysts, 110 °C reaction temperature, and 1:9 molar ratio of glycerol to acetic acid. Copyright © 2024 by Authors, Published by BCREC Publishing Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).
Co-Authors Herry Purnama, Herry Luh Putu Ratna Sundari Marwan Effendy Mastuti, Isnadiah Endang Nur Hidayati Pambudi, Wahyu Devi Satna