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All Journal Indian Journal of Forensic Medicine & Toxicology
Jalal Hasan Mohammed1, Alaa Jawad Kadhim2, Nagham Mahmood Aljamali3
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Thiophene-Cyclic and Sulfazane Derivatives (Preparation, Spectral Analysis, the Behavior in Organic Solvents, Microbial Testing) Jalal Hasan Mohammed1, Alaa Jawad Kadhim2, Nagham Mahmood Aljamali3
Indian Journal of Forensic Medicine & Toxicology Vol. 14 No. 2 (2020): Indian Journal of Forensic Medicine & Toxicology
Publisher : Institute of Medico-legal Publications Pvt Ltd

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.37506/ijfmt.v14i2.3166

Abstract

The thiophene core is the most broadly applied constructing blocks to the production of many biomolecules ,pharmaceutical drugs ,vitamins ,also in industrial compounds, in dyes compounds because of its high stability in environment. Thiophene derivatives were synthesized in present study from chalcone compound as a starting material from aldol reaction in first step, followed by cyclization reactions by using various conditions, and this paper involved new reaction for diazonium salts to producing (Sulfide- azo) compounds in same bond for the first time that we termed (Sulfazane) as a first and Novel preparation to this new type of compounds.,the synthesized derivatives were confirmed through numerous spectral techniques (FT.IR ,H.NMR ,C.NMR), other physic-chemical data for synthesized thiophene derivatives ,besides to studying of behavior of compounds in organic solvents and screening tests for efficiency of thiophene derivatives against microbes
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